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Ms. Joan Kessner 2 March 7, 1991 WHC-SD-EN-TI-136, Rev. 0 -- 2 Semi-Volatiles: BNA The samples were not extracted within the prescribed holding time, missing the seven (7) day holding time for extraction by seven (7) days. Once extracted, the samples were analyzed within the prescribed holding time. All surrogate standards criteria were within percent recovery acceptance limits. All DFI'PP tune criteria were within acceptance criteria. All "CCC" and "SPCC" components met acceptance criteria for both the initial and continuing calibration check samples. All internal standard areas were within acceptance criteria. All matrix spikes and matrix spike duplicates were within the acceptance requirements. All the samples were analyzed within the prescribed holding times. All surrogate standards criteria were within percent recovery acceptance limits. All Bra tune criteria were within acceptance criteria. All CCC and SPCC components net acceptance criteria for both the initial and continuing calibration check sample. All internal standard areas were within acceptance criteria. All matrix spikes and matrix spike duplicates were within the acceptance requirements. I certify that this data package is in compliance with the terms and conditions of the OSM' s revised Statement of work and letter dated December 20, 1990, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. . Morrow Department manager Analytical Chemistry Department (K-25) Attachments cc/attach: D.*L .Auiburgey S.R.smith - RC cc: N.P.Buddin S .W.Goza H.H. Sullivan D-188 Sincerely, Deborah L. Amburgey Program manager <strong>Hanford</strong> Support Program Clarence R. Kirkpatrick Program Manager Waste Management Analysis
WHC-SD-EN-TI-1 36 , Rev. 0 a" Ridge K-25 <strong>Site</strong>5 Analytical Chemistry Department-5 Results of Analyses sauls 10: "0122"-51. pro ject: 01.32 027S customer Seeple ID: 27-1.02 Cutomer: KSinSU M Requisition Nmber: oate Sampled: 16S-0C=21990 Date Ss~2. Received: 20-DEC-1990 samp.ed By: Date Sseple completed: 27-JAII-1992. material Descrition: SOIL (3 Result has been Corrected for Spike Date Ac0%v mnber Proceduare go. Analysis Result Daits AnalystPiem r Colte 1.02003 ZPA-3050 lad
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SUPPORTING DOCUMENT 1. Total Pages
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Dae Reced INFORMATION RELEASE REQUE
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INTRODUCTION WC-SD-EN-TI-136, Rev.
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P.O. Box 1970 Rfichland. WA 99352 W
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