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WC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS ID: 901206-023 Customer Sample ID: W-105 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 10652 Sample Matrix: SOIL Instrument ID: 5970513 Requfsition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BRA - lase/NeutraL/Acid Compounmds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Number: Analysis Procedure Numb~er: RNA (CIP) NOP Percent Moisture: 5.0 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 GA File Number: MA 11:Result has been Corrected f or Spike CAS ug/Kg CAS ug/Kg .................................. .......... ........... .............................. .......... 108-95-2 Phenol 980U 106-47-8 4-Chtoroanitine 980U 111-44-4 bisc2-ChLoroethyl)ether 980U 87-68-3 Hexachlorobutadiene 980U 95-57-8 2-Chlorophenot 980U 59-50-7 4-Chloro-3-methyiphenot 980U 541-73-1 1,3-DlchLorobenzene 9B0U 91-57-6 2-1MethylnaphthaLene 980u 106-46-7 1,4-Dlchiorobenzene 980U 77-47-4 Nexachtorocyctopentadiene 98OU 100-51-6 *enzyl Alcohol 980U 88-06-2 2,4,6-TrichlorophenoL 980u 95-50-1 1,2-Dichlorobenzene 981. 95-95-4 2,4.5-Trichlorophenol 4700u 95-48-7 2-MethyiphenoL 980U 91-58-7 2-ChLoronaphthalene 98Ou 108-60-1 bis(2-ChloroisopropyL)ether 980U 88-74-4 2-NitroaniLine 4700U 106-44-5 4-MethylphenoL 980U 131-11-3 DimethyiphthaLate 980U 621-64-7 N-Nitroso-di-n-propylamine 980U 208-96-8 Acenaphthylene 980U 67-72-1 Hexachioroethane 981. 99-09-2 3-Nitroaniline 4700u 98-95-3 Hitrobenzene 9B0U 83-32-9 Acenaphthene 981. 78-59-1 Isophorone 9B0U 51-28-5 2,4-Dinitrophenol 4700U 88-75-5 2-Nltrophenot 981. 100-02-7 4-NitrophenoL 4700u 105-67-9 2,4-DimethylphenoL 981. 132-64-9 Dlbenzofuran 980U 65-85-0 Benzoic Acid 4780 -~.~rLA 121-14-2 2,4-Dinitrotoluene 980U 111-91-1 bis(2-Chtoroethoxy)methane 9801) 606-20-2 2,6-Dinitrototuene 980U 120-83-2 2,4-DichLorophenoL 98OU 84-66-2 Diethylphthalate i20 46e~e LA 120-82-1 1,2,4-Trichlorobenzene 9801. 7005-72-3 4 -Chi orophenyL -phenyl ether 980U 91-20-3 Naphthatene 981. 86-73-7 FLuorene 980U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO Not detected. A - ALdol condensation product. D - Secondary dilution. 7 E - Exceeds initial calibration range. D-32
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS 1D: 901206-023 Customer Sample tD: N-105 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File to: 10652 Sample Matrix: SOIL Instrument t0: 597093 Requisition Number: Authorized Bly: D. C. Canada Date Sample Received: 6-DEC- 1990 BRA - *ase/Meutral/Acid Compounds CTCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Numb~er: Analysis Procedure Number: BRA CCLP) HOP Percent Moisture: 5.0 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Stank: 901213-028 QA File Numb~er: NA 11 : Result has been Corrected f or Spike CAS ug/Kg CAS ug/Kg 100-01-6 4-Nftroanitlne 4700t) 53-70-3 Dibenz(a~h)anthracene 98OW 534-52-1 4.6-Dinitro-2-methytphenot 4701U 191-24-2 *enzo(g.h.l)perylene 9S0U 86-30-6 -Ntrosodlphenytmlne 980U 101-55-3 4-Bromophenyl-phenylether 9BOU 118-74-1 Hexachlorobenzene 980U 87-86-5 Pentachtorophenot, 470OU 85-01-8 Phenanthrene 98OU 120-12-7 Anthracene 980U 84-74-2 Di-n-butylphthalate 3600s,.. LA. 206-44-0 Fluoranthene 98WU 129-00-0 Pyrene 98Wu 85-68-7 UutylbenzyLphthalate 98WU 91-94-1 3,3'-DichLorobenzidine 200WU 56-55-3 genzo(a)anthracene 98WU 117-81-7 bis(2-Ethythexyt)phthaLate "ede 5 ,50 (A. 218-01-9 Chrysene 98WU 117-84-0 Di-n-octylphthatate 98WU 205-99-2 *enzo(b)fluoranthene 98WU 207-08-9 Benzo~kfLuoranthene 98W ' ( 50-32-8 Senzo(a)pyrene 98WU 193-39-5 lndenoCl,2,3-cd)pyrene 98WU Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numb~er is the attainable detection limit for the sample. B - Analyte was foun~d in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - AldoL condensation product. O - Secondary dilution. E - Exceeds initial calibration range. D-33
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P.O. Box 1970 Rfichland. WA 99352 W
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