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WIIC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 2 AnaLIS ID: 901206-024 Customer Sample ID: N-106 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 10653 Sample Matrix: SOIL Instrument ID: 597013 Requisition Numb~er: Authorized By: 0. C. Canada Date Sample Received: 6-OEC-1990 BRA -Base/Neutral/Acid Compounds CTCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Numiber: Analysis Procedure Number: BRA (CLP) MOP Percent Moisture: 3.3 Dilution Factor: 2.0 Percent Moisture (decanted): Analyst: C M4EEHAN Associated Blank: 901213-028 GA File Number: NA I]:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 108-95-2 Phenol 2000U) 106-47-8 4-ChtoroaniLine 20001U 111-44-4 bis(2-Chtoroethyt)ether 2000t) 87-68-3 Nexachtorobutadiene 200OU 95-57-8 2-ChlorophenoL 200OU 59-50-7 4-Chlora-3-methylphenoL 200OU 541-73-1 1,3-Dichlorobenzene 200013 91-57-6 2-Methyinaphthalene 2000u 106-46-7 1,4-Dichlorobenzene 20001U 77-47-4 HexachLorocyclopentadiene 2000t3 100-51-6 Benzyl Alcohol. 20001U 88-06-2 2,4.,6-Trichlorophenot 20001U 95-50-1 1,2-DichLorobenzene 20003 95-95-4 2.4,5-Trichtorophenol 9501U 95-48-7 2-MethytphenoL 2000t3 91-58-7 2-ChloronaplithaLene 2000u 108-60-1 bisC2-Chloroisopropyl)ether 20001U 881-74-4 2-Nitroaniline 9500U3 106-"4-5 4-MethyLphenol 2000t3 131-11-3 DimehylphthoLate 2000t) 621-64-7 -Nitroso-di-n-propylamine 20001U 208-96-8 Acenaphthylene 200013 67-72-1 Hexachloroethane 2000U 99-09-2 3-Nitroaniline 950013 98-95-3 Nitrobeniene 200013 83-32-9 Acenaphthene 20001U 78-59-1 Isophorone 200013 51-25-5 2,4-DinitrophenoL 950013 88-75-5 2-Nitrophenol 2000t3 100-02-7 4-Nitrophenol 950013 105-67-9 2,4-DimethytphenoL 20001U 132-64-9 Dibenzofuran 20001U 65-85-0 Benjoic Acid 950OU 121-14-2 2,4-Dinitrotoluene 20001U 111-91-1 bis(2-Chloroethoxy)methane 20001U 606-20-2 2,6-Dinitrotoluenve 2000u3 120-83-2 2,4-Dichlorophenol 20001U 84-66-2 Diethytphthalate 2oaa 25e~O do .. 120-a2-1 1,Z,4-Trichlorobenzene 200013 7005-72-3 4-ChtorophenyL-phenylether 20001U 91-20-3 Naphthalene 20001U 86-73-7 Fluorene 2000u3 Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. 8 - AnaLyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - Aldol. condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-36
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLiS ID: 901206-024 Customer Sample ID: N-106 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File 10: 10653 Sample Matrix: SOIL Instrument ID: 597003 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BNA -Base/NeutraL/Acid Compounlds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Numb*er: Analysis Procedure Number: DNA CCLP) MOP Percent Moisture: 3.3 Dilution Factor: 2.0 Percent Moisture (decanted): Analyst: C MEENAN Associated Blank: 901213-028 CA File Number: NA 0 : Result has been Corrected f or Spike CAS ug/Kg CAS ug/K9 100-01-6 4-Nitroanitine 950OU 53-70-3 Dibenz(a~h)anthracene 200OU 534-52-1 4,6-Dlnitro-2-mthytphenoL 950OU 191-24-2 Benzo(g,h~i)peryLene 2000U 86-30-6 N-itrosodiphenylamine 200OL! 101-55-3 4-Dromopheny-phenylether 200OU 118-74-1 Hexachtorobenzene 2000U 87-86-5 PentachtorophenoL 9500U 85-01-8 Phenanthrene 2000U 120-12-7 Anthracene 2000U 84-74-2 Di -n-butytphthalate 2000'S.. LA 206-44-0 Fluoranthene 200DU 129-00-0 Pyrene 200WU 85-68-7 Dutylbenzylphthalate 200OU 91-94-1 3,3'-Dichiorobenzidine 390WU 56-55-3 Denzo(a)anthracene 200WU 117-81-7 bis(2-Ethythexyt)phthatate 2500 S, LA 218-01-9 Chrysene 2000t 117-84-0 Di-n -octytphthatate 110 J ,4 205-99-2 Benzo~b)ftuoranthene 200WU 207-08-9 Denzo(k)fLuoranthene 2000W 50-32-a Denzo(a)pyrene 280 .1 193-39-5 Indeno(1,2,3-cd)pyrene 320 J Data Reporting Qualifiers: U - Comrpound was analyzed for but not detected. The number is the attainable detection limit for the samrple. B - Analyte was found in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO - Mot detected. A - AldoL condensation product. 0 - Secondary dilution. E - Exceeds initial calibration range. D-37
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