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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 naLIS ID: 901206-046 Customer Sample ID: U-124 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: >14475 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Numer: Authorized Dy: D. C. -Canada Date sample Received: 5-DEC-1990 BNA - Base/Neutral/Acid Compounds CTCL) Date Extracted/Prepared: 13-DEC- 1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Number: Analysis Procedure Number: DNA (CIP) NDP Percent Moisture: 7.1 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Dlank: 901214-083 OA File Numrber: NA U:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ..............................................----------.............................. .......... 100-01-6 4-Nitroaniline R 4800UJ 53-70-3 Oibenz(a~h)anthracene R 1000u 534-52-1 4,6-Dinitro-2-methylphenot R 48D0U 191-24-2 Denzo(gh,I)perytene R 1000U 86-30,6 N-Nltrosodlphenylamine ft 1000U 101-55-3 4-Dromophenyl-phenytether Rt 1000U 118-74-1 Hexachlorobenzene ft IOOOU 87-86-5 PentachlorophenoL ft 4800U 85-01-8 Phenanthrene ft 1000U 120-12-7 Anthracene R 1000U 84-74-2 0l-n-butytphthatate 3700'ts, Lt. 206-44-0 FLuoranthene ft 1000.3 129-00-0 Pyrene ft 1000U 85-68-7 Dutylbenzylphthalate ft 1000tU 91-94-1 3,3'-DichLorobenzidine R 2000U 56-55-3 Denzo~a)anthracene ft 1000U 117-81-7 bis(2-Ethylhexyt)phthaLate ft 1000U / 218-01-9 Chrysene R 1000U 117-84-0 Di-n-octylphthatate ft 1000U 205-99-2 Benzo(b)fluoranthene ft 1000UI 207-08-9 Denzo(k)fluoranthene ft 1000U 50-32-8 Denzo(a)pyrene ft 1000U 193-39-5 Indeno~l.2,3-cd)pyrene Rt 1000U Data Reporting Qualifiers: V /? U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. 9 - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-110
WIlC-SD-EI-TI-136, Rev. ') Oak Ridge K-25 <strong>Site</strong> Anal ytical Chemistry Department INA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-046 Customer Sample 10: N-124 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL Fite ID: ),14475 Level: (low/med): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. 7.1 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxH pH: ____ GPC Cleanup: (Y/N) N Concentration Units Nuber TICs found: 20 Cug/L or uglKg): u2LK2 CAS NUMBER COMPOUND NME RT IEST. CONC. a ~ O ~ 1. I2. I3. I4. 123-42-21 2-Pentanone. 4-hydroxy-4-methy 1 UNKNONW ALCOHOL 1 UNKNOWN ALCOHOL 1 UNKNOWN 6.! I Q18 +6i; 2 "A-u 66 8J ~ 3000 in~ - Me H3~ I5. I6. I7. 8. 1 UNKNOWN 1 UNKNOWN 1 UNKNOWN 1 UNKNOWN HYDROCARBON ~ 1?.ee I 10I.I 19,10I 7OOI ~ 288 Z500 4-46-~ M .oIS 658oI 9. [UNKNOWN PHTHALATE ESTER N .6?. 1. I10. IUNKNOWN HYDROCARBON I 24.84 I1500I 11. IUNKNOWN HYDROCARBON 22.090 I12. IANTHRACECOIONE 28e i 1OOis .D 13. [UNKNOWN HYDROCARBON ?63 8 0I. 14. [UNKNOWN HYDROCARBON N9T.66 1 leg d . 15. UNKNOWN HYDROCARBON ?0Z.;c4 XCOG.I ' 16. ______jUNKNOWN ALKOXY COMPOUND I cy.se F 0 IJ I17. jUNKNOWN HYDROCARBON 1 29.80 1 2100 j. 18. UNKNOWN HYDROCARBON i n RA iOj4. 19. UNKNOWN HYDROCARBON 34~.68 6;90o~ 20. jUNKNOWN ALKOXY COMPOUND j 37.26 j1200 j 1 121.1__ _ _ _ _ _ _ _ _ _ j__ _ _ __ _ _ I__ _ 122.111__ _ _ 1__ _ 123.1__ _ _ _ _ _ _ _ _ _ __ _ _ 1__ _ _ 1__ _ 124. I 125. II 126. I I 127. II 128. I 129.I I 130. II Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J Indicates an estimated value. RD -Not detected. A - AldoL condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P-Probable identification. D-111
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