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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department INA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-019 Custmer Samrple 1D: N-101 Laboratory: Organic MassSpectroscopy Laboratory Customer: J1. KESSNER/R. SNUCK Sample Matrix: SOIL File ID: 10646 Level: (tow/med): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 13-DEC-1990 % Moisture: not dec. 5.7 dec. _____Date Extracted: 12-DEC-1990 Extraction: CSepF/Cont/Sonc) SoxH PH*: GPC Cleanup: CT/N) N Concentration units Number TICs found: 15 (ug/L or ug/Kg): uqK I CAS NUMBER C01MPOUND NAME I RT EST. CONC. a I1. 123-42-21 2-Pentenone, 4-hydroxy-4-mothy 5 .9i i aCI"I 2. 872-50-41 2-Pyrrotidinone. 1-methyl- 9 .81! -44 -B I3. 1 Unknown 1 12.50! goo1 I4- 25013-16-51 Phenot.(1.1-dimethylethyl)-4-m I5. Unknown 4 6.L 4; mee1 ----- 6. IUnknown I7._17851-53-51 1.2-genzenedicarboxylic acidb j.3 Wes0 IWag --oul t ~ I 8. I Unknown (Hydrocarbon) .2~i.6 - -4-4 -- I I9. 10. I11. IUnknown IUnknown (Hydrocarbon) IUnknown I I 21.96 J420 23.74 J590 24.11 J570 1 1 I 1 1 12.______ Unknown (sat'd Hydrocarbon) 13. Unknown (sat'd Hydrocarbon) I14. jUnknown (Hydrocarbon) I15. fUnknown (sat'd Hydrocarbon) 116. I I A .6i- 149t 27.78 I2100 i-O.3 -tmI JB inn 1 4_1 1~ -9 ___ I 17. ___I is8. ____IL___I 1'9._____III__ _ 120.--II __ 121. ___________________ 1 __ I 22.II I 123.I I 124.--- I 125. ___________________1II 126. I 127. I I 128.II I 129.--I 130.I I Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B Analyte was foun~d in the reagent blank as well as the sample. J1 - indicates an estimated value. NO - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds Initial calibration range. P - Probable Identification. D- 18
WfIC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 1 AnaLIS ID: 901206-019 Customer Sample 10: N-101 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07606 Sample Matrix: SOIL Instrument 10: 597012 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VOA -Volatile Organic Compounds CTCI) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Number: VOkA (CP) MOP Percent Moisture: 6 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL HL3DLESTOM Associated Slank: 901211-004 CA File Number: MA 0l : Result has been Corrected for Spike CAS uglKg CAS ug/Kg 74-87-3 Chloromethane 11U 79-00-5 1.1,2-Trichtoroethane 5U 74-83-9 Uromomethane 1Ut 71-43-2 Benzene 5u 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichtoropropene 5U 75-00-3 Chloroethane 11t) 75-25-2 Bromoform 5u 75-09-2 MethyLene Chloride 5U 108-10-1 4-Nethyt-2-pentanone 11U 67-64-1 Acetone 11U 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disuifide 5U 127-18-4 Tetrachtoroethene 5u 75-35-4 1*1-Dfchtoroethene SU 79-34-5 .1.1,2.Z-TetrachLoroethane 5U 75-34-3 1 1 1-Dichtoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichioroethene (total) SU 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform .5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Oichioroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1*1-Trichtoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichtoromethane 5U 78-87-5 1,2-Dichioropropane 5U 10061-01-5 cis-1,3-Dichloropropene 5U 79-01-6 Trichtoroethene 5U 124-48-1 Dibronwchtoromethane sU Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The nwiber is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J -Indicates an estimated value. NO - Not detected. A - Aldot condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D- 19
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