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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLlS ID: 901206-036 Customer Sample ID: M-116 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSMER/R. SNUCK File ID: 304465 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Numb~der: Authorized By: D. C. Canada Date Sample Received: 5-DEC-1990 BHA - Base/Neutral/Acid Comp~ounds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAM-1991 Preparation Procedure Nuber: Analysis Procedure Number: BNA (CLP) MOP Percent Moisture: 6.3 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 CA File Nu.mber: MA U:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 108-95-2 Phenol ft 9901) 106-47-8 4-Chloroanitine ft 99011 111-44-4 bis(2-Chloroethyt)ether ft 9901) 87-68-3 Nexachlorobutadiene ft 9901) 95-57-8 2-Chtorophenot ft 9901) 59-50-7 4-Chloro-3-methylphenot ft 9901) 541-73-1 1,3-Dichtorobenzene R 9901) 91-57-6 2-MethylnaphthaLene Rt 9901) 106-46-7 1,4-Dichlorobenzene R 9901) 77-47-4 Hexachlorocyclo pen tadiene R 99011 100-51-6 Benzyl Alcohol ft 9901) 88-06-2 2,4,6-Trichtorophenot R 9901) 95-50-1 i,2-Dichlorobenzene ft 9901) 95-95-4 2,4,5-TrichLorophenol R 48001) 95-48-7 2-Methytphenol R 9901) 91-58-7 2-Chtoronaphthatene R 9901 108-60-1 bis(2-ChLoroisopropyt)ether R 9901) 58-74-4 2-Nitroaniline ft 480011 106-441-5 4-Methylphenot ft 9901) 131-11-3 Dimethylphthalate ft 9901) 621-64-7 N-mitroso-di-n-propyiamine R 9901) 208-96-8 Acenaphthylene ft 9901) 67-72-1 Hexachtoroethane R 9901) 99-09-2 3-Nitroaniline R 48001) 98-95-3 Mitrobenzene R 991. 83-32-9 Acenaphthene, R 991. 78-59-1 Isophorone R 991. 51-28-5 2,4-Dinitrophenol Rt 480011 88-75-S 2-Nitrophenol ft 9901) 100-02-7 4-Nitrophenol ft 4801U 105-67-9 2.4-Di 'methylphenot Rt 9901) 132-64-9 Dibenzofuran Rt 99011 65-85-0 Benzoic Acid ft 48001) 121-14-2 2,4-Dinitrotoluene R 99011 111-91-1 bisC2-Chloroethoxy)methane R 9901) 606-20-2 2,6-Dinitrotoluene ft 9901 120-83-2 2,4-Dichlorophenol ft 9901) 84-66-2 Diethylphthatate ft 9901 120-82-1 1,2,4-Trichtorobenzene R 9901) 7005-72-3 4-Chlorophenyl-phenytether Rt 99011 91-20-3 Naphthalene ft 9901) 86-73-7 Fluorene ft 9901 Data Reporting Qualifiers: U - Comrpound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the saple. J3 - Indicates an estimated value. RD - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D- 74
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-036 Customer Sample ID: N-116 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 314465 Sample Matrix: SOIL Instrument ID: RP-5985 Rtequisition Number: Authorized By: 0. C. Canada Date Sample Received: 5-DEC-1990 DNA - Base/Neutral/Acid Compounds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Nuber: Analysis Procedure Number: 3INA (CLP) NOP Percent Moisture: 6.3 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 GA Fite Number: NA 11:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .......................... .......... ........... .............................. .......... 100-01-6 4-Nitroaniline ft 4800U 53-70-3 Dibenz~a,h)anthracene ft 990U 534-52-1 4.6-Dinitro-2-methylphenot ft 480OU 191-24-2 Benzo(g~h,i)perylene R 990U 86-30-6 N-itrosodfphenylamine ft 990U 101-55-3 4-Bromophenyl-phenylether ft 990U 118-74-1 Hexachlorobenzene ft 990U 87-86-5 PentachlorophenoL ft 4800U 85-01-8 Phenanthrene ft 990U 120-12-7 Anthracene Rt 990U 84-74-2 Di-n-butylphthaLate 2900-1, Lk. 206-44-0 Fluoranthene ft 99OU 129-00-0 Pyrene ft 990U 85-68-7 Butylbenzylphthalate Rt 99OU 91-94-1 3,3'-Dichlorobenzidine Rt 2100U 56-55-3 Benzo~aanthracene ft 990U 117-81-7 bisC2-Ethythexyl)phthalate R 990U 218-01-9 Chr-ysene ft 990U 117-84-0 Di-neoctylphthalate ft 990U 205-99-2 Benzo(b)fluoranthene ft 990U 207-08-9 Benzo(k)fLuoranthene ft 990U 50-32-8 Benzo(a)pyrene ft 99U 193-39-5 Indeno(1,2,3-cd)pyrene ft 99OU Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. 8 Analyte was found in the reagent blank as well as the sample. .1 -indicates an estimated value. ND -Not detected. A -Aldol condensation product. D Secondary dilution. E -Exceeds initial calibration range. D-75
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P.O. Box 1970 Rfichland. WA 99352 W
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