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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-045 Customer Sample ID: M-123 Laboratory: Organic mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: ),14474 Sample Matrix: SOIL Instrument ID: MP-5985 Requisition Numiber: Authorized By: 0. C. Canada Date Samp~le Received: 5-DEC-1990 SNA - Base/Neutral /Acid Compyounmds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Numiber: Analysis Procedure Number: INA CCLP) NDP Percent Moisture: 8.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 OA File Numiber: NA C]:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ------. . ............-----.------- .------.*................ ............................. .......... 100-01-6 4-Nitroaniline R 520OU 53-70-3 Dibenz(a,h)anthracene R IODOU 534-52-1 4,6-Dinitro-2-methylphenoL R 5200U 191-24-2 Benzo(g,h,i)perylene R I 00OU 86-30-6 N-Nitrosodiphenytomine R 1000U 115-3 4-Blromophenyl-plienylether R 1000U 118-74-1 Hexachlorobenzene R 100OU 87-86-5 Pentachtorophenol R 520OU 85-01-5 Phenanthrene R 1000U 120,12,7' Anthracene R 1000U a4-74-2 Di-n-butytphthalate 33001... Lk. 206-44-0 Fluoranthene, R 100OU 129-00-0 Pyrene R 100OU 85-6a-7 Butylbenzylphthalate R 1000U 91-94-1 3,3'-Dichtorobenzidine R 2100U 56-55-3 Uenzo~a)anthracene R 1000U 117-81-7 bis(2-Ethythexyl)phthatate R 1000U 218-01-9 Chrysene, R 1000U 117-84-0 Di-n-octylphthalate R 1000U 205-99-2 Benzo(b)fluoranthene R 100OU 207-08-9 Benzo(k)fluoranthene R 1000U 50-32-8 Benzo(a)pyrene R 1000U 193-39-5 Indeno(1,2,3-cd)pyrene R 1000U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numaber is the attainable detection limit for the sample. B - Analyte was founid In the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-106
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department INA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-045 Customer Sample ID: N-123 Laboratory: Organic Mass Spectroscop~y Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: 3,14474 Level: (low/mad): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. 8.5 dec. _____Date Extracted: 13-DEC-1990 Extraction: CSepF/Cont/Sonc) SoxH PH: ____ GPC Cleanup: (YIN) Nj Concentration Units Number TICs founid: 20 Cug/L or ug/Kg): _tsgK2 CAS NUMBER COMPOUND NAME RT EST. CONC. I1. 123-42-21 2-Pentanone. 4-hydroxy-4-methy 2. 1 UNKNOWN I3.1 UNKNOWN ALCOHOL I .65- --- iOfl0 - 15.721 95011 J 438 07 --- I d9 - I~e 4 .___ _ 1 UNKNOWN 10.90I No"I do I5. 6. I7. jUNKNOWN JUNKNOWN jUNKNOWN I 19.0 i9.?e I40 20!.90 I3e 3neOIJ ! d I~ d9o I de a . 9. jUNKNOWN HYDROCARBON 1UNKNOWN PHTHALATE ESTER I 3.7 f I -?*-~ 60 -~ I11. IUNKNOWN HYDROCARBON I, jt- I 1 2. I13. 14. IANTHRACECOTONE IUNKNOWN HYDROCARBON IUNKNOWN HYDROCARBON I65 I I j I Q00 9; d o i IM)0 I . I15. IUNKNOWN HYDROCARBON 2e.7 F9 -"GO Ie- 16. IUNKNOWN ALKOXY COMPOUND j -9.159O 17. IUNKNOWN HYDROCARBON 29.81 I2900 .1 18. IUNKNOWN HYDROCARBON I 3 0.85, C o--o 19. I20. UNKNOWN HYDROCARBON IUNKNOWN HYDROCARBON I 5l.?V ;8700 I " nan.7I 121. II___ 122. II___ 123. IIIJ___ 124. J__ _ 125. III___ 126. III___ 127. I __ _ I 28.IIJ__ _ 129. IIJ___ 130.I I Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The numb~er is the attainable detection Limit for the sample. B8 Analyte was found in the reagent blank as well as the sample. J Indicates an estimated value. ND -Not detected. A Aldol condensation product. D Secondary dilution. E -Exceeds initial calibration range. P -Probable Identification. D-107
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