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WIIC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS 10: 901206-025 Customer Sample ID: N-107 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File 1D: 10654 Sample Matrix: SOIL Instrument ID: 597003 Requisition Neuber: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BNA - Ease/Neutral/Acid Compounds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Numb~er: Analysis Procedure Number: BNA CCLP) MOP Percent Moisture: 5.0 Dilution factor: 1.0 Percent Moisture (decanted): Analyst: C MEENAN Associated Btank: 901213-028 GA Fite Number: NA El Result has been Corrected f or Spike CAS ug/Kg ............................ .......... CAS ug/Kg ........... .............................. .......... 108-95-2 Phenol 100OU 106-47-8 4-ChLoroaniLine 100OU 111-44-4 bisC2-Chloroethyt)ether 100OU 87-68-3 Nexachlorobuatadiene 10O0u 95-57-8 2-Chlorophenol 1000U 59-50-7 4-Chtoro-3-methyLphenot 1000U 541-73-1 1,3-Dichlorobenzene 1000U 91-57-6 2-NethylnaphthaLene I 000U 106-46-7 1,4-Dichtorobenzene 1000U 77-47-4 Hexachiorocyclopentadiene 1000U 100-51-6 BenzyL Alcohol 100OU 88-06-2 2,4,6-Trichlorophenol 1000U 95-50-1 1,2-Dichlorobenzene 100OU 95-95-4 2.I..5-TrichtorophenoL 490OU 95-48-7 2-Methyiphenol 100OU 91-58-7 Z-Chloronaphthatene 1000U 108-60-1 bisC2-ChtoroisopropyL)ether 1 00OU 88-74-4 2-Nitroanline 4900U 106-44-5 4-Methyiphenol I 00OU 131-11-3 Dimethylphthalate 1000U 621-64-7 N-N itroso-di-n-propyLamine I 00OU 208-96-8 Acenaphthylene 100Ou 67-72-1 Hexachtoroethane 100OU 99-09-2 3-Nitroaniline 490OU 98-95-3 Nitrobenzene 1000U 83-32-9 Acenaphthene 1000U 78-59-1 Isophorone 1000U 51-28-5 2,4-DinitrophenoL 4900U 88-75-5 2-Nitrophenol IOOOU 100-02-7 4- N it rophenolI 490OU 105-67-9 2,4-Dimethytphenot 1000U 132-64-9 Dibenzofuran l0OUt 65-85-0 Uenzoic Acid /066 43096 Ue( 121-14-2 2,4-Dinitrotoluene 1000u 111-91-1 bisc2-Chloroethoxy)methane 1000U 606-20-2 2,6-Dinitrotoluene 1000u 120-83-2 2,4-DichlorophenoL 1000U 84-66-2 DiethylphthaLate fo00 238-~- do 120-82-1 1,2,4-Trichlorobenzene 1 000U 7005-72-3 4-Chlorophenyt-ph eny tether 1000U 91-20-3 Naphthalene 1000U 86-73-7 Fluorene 1000U Data Reporting Qualifiers: 4 U - Compound was analyzed for but not detected. The numb~er Is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO - Not detected. AlAdol condensation product. D - Secondary dilution. e E-Exceeds initial calibration range. D-40
WNC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLlS 10: 901206-025 Customer Sampte ID: N-10? Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite 10: 10654 Sample Matrix: SOIL Instrument 10: 597013 Requisition Number: Authorized By: 0. C. Canada Date Sample Received: 6-DEC-1990 BNA -Base/Neutral/Acid Compounds CTCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Numb~er: Analysis Procedure Number: DNA (CLP) HOP Percent Moisture: 5.0 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 OA File Numb~er: NA U] : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 100-01-6 4-Nitroanitine 4900U 53-70-3 Dibenz(a~h)anthracene IOOOU 534-52-1 4,6-Dinitro-Z-methytphenot 4900U 191-24-2 Senzo(g~hJi)perytene 100OU 86-30-6 N-Nitrosodlphenylaamine 1000U 101-55-3 4-Bromophenyl-phenytether IOOOU 118-74-1 Hexachtorobenzene 1000U 87-56-5 Pentachlorophenol 4900U 85-01-8 Phenanthrene 100OU 120-12-7 Anthracene 1000U 84-74-2 Di-n-butyLphthalate 3300-S. LA' 206-44-0 Fluoranthene 1000U 129-00-0 Pyrene 91 .1 85-68-7 Butytbenzylphthatate 1000U 91-94-1 3,3'-Dichlorobenzldine 200OU 56-55-3 Benzo~aanthracene 100OU 117-81-7 bis(2-Ethythexyt)phthaiste 439 ds /000 Lk 218-01-9 Chrysene 1000U 117-84-0 Di-n-octytphthatate 100OU 205-99-2 Benzo(b) f uoranthene i000U 207-08-9 Denzo(k)fluoranthene 50-32-8 Uenzo(a)pyrene 193-39-5 lndeno(1,2,3-cd)pyrene Data Reporting Qualifiers: 1000U i000U 1000u / U -Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. 8 - Analyte was found in the reagent blank as welt as the sample. i Indicates an estimated value. NO - Not detected. A -Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-41
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P.O. Box 1970 Rfichland. WA 99352 W
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