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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department lilA (CL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS I0: 9"1206-035 Customer Sample 10: N1-115 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL Fite 1D: 10664 Level: Clow/med): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % moisture: not dec. - 4.8 dec. _____Date Extracted: 12-DEC-1990 Extraction: (SepF/Cont/Sonc) Soxl pM: ___ GPC Cleanup: (T/N) N Concentration Units Number TICs found: 14. (ugIL or ug/Kg): _uU ICAS NUMBER ICOMPOUND NAME I 332sg~zzU3Uu j 322:uz~~uuzm I1. 123-42-21 2-Pentanone, 4-hydroxy-4-methy I2. 872-50-41 2-Pyrrolidinone, 1-methyl- 3. 1 unknown I4. 25013-16-51 Phenol,(l.1-dimethytethyl)-.-m AT EST. CONC. j I ax2azza2zu22 .zZ: W=j =ZZmZ I .9; I 270-09 - 9 .00 I tip 1 j 12.521 600 J q 6-5..It~I~ I5. Unknown (Alkyt Hydrocarbon) j l... I40 6. IUnknown (Alkyl Hydrocarbon) 23 n ~ *4 d! I zuuum*zu I7. Iunknown (sat'd Hydrocarbon) I8.- 17851-53-51 1.2-Benzenedicarboxytic acid.b I9. 123-79-51 Dioctyl Adipate 10. IUnknown (sat'd Hydrocarbon) I56 j 25.97 1570 j 26.38 I1600 I 6.'f I IJ 78I -1" / / q I 11. I12. 13. IUnknown IUnknown (Alkyl Hydrocarbon) IUnknown (sated Hydrocarbon) j 27.79 I1700I -20.4E I -7O I JO 32.59 390 4____ 114. 115. IUnknown j I__ _ 33.73j _ _ i__ _ _ 380 _ _I_ _ _ J16.II__ 117.I __ _ _ _ _ _ _ __ __ _ _ _ _ _ _ _I_ _I_ _ _ _ _ I 18. 119. II_ _______I_______I___ _ _ _ _ _ _ _ _ _I_ _ _ _ 120. II_ _ _ _ _ _ _ _ _ _I_ _ _ 21. II_ _ _ _ _ _ _ _ _ _I_ _ _ 122. II_____ _____ ___ 123.II__ _ _ _ __ _ _ _ _I_ _ _ I 124.IIJI 125.I III 126.I II 127.II I 128. I I 129. I II 130. I II Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection Limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. D -Secondary dilution. E - Exceeds initial calibration range. P - Probable identification. D-72
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of I AnaLIS ID: 901206-035 Customer Sample 10: N-115 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSMER/R. SHUCK File ID: 07619 Sample Matrix: SOIL Instrum~ent 10: 59702 Requisition Number: Authorized By: 0. C. Canada Date Samiple Received: 6-DEC- 1990 VOA -Volatile organic Comp~ounds CTCL) Date Extracted/Prepared: Date Analyzed: 1-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Numb'~er: VGA (CLP) MOP Percent Moisture: 5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL HUDOLESTON Associated Blank: 901211-004 @A File Nmiaber: MA 11 : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ............................... .......... ........... .............................. .......... 74-87-3 Chloromethane 11U 79-00-5 1,1.2-Trichloroethene 5U 74-83-9 Bromomethane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 111U 10061-02-6 trans-1.3-Oichloropropene SU 75-00-3 Chloroethane 11U 75-25-2 Iromoform 5U 75-09-2 Methylene, Chloride 511 108-10-1 4-Methyl-2-pentenone 11U 67-64-1 Acetone 34 LA 591-78-6 2-Hexanone 111) 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachloroethene 5U 75-35-4 1.1-Dichloroethene SU 79-34-5 1,1,.2-Tetrachioroethane 5U 75-34-3 1,1-Dichloroethane 5U 108-08-3 Toluene 5U 540-59-0 1.2-Dichioroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzeie 5U 107-06-2 1,2-Dichtoroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 1IU 1330-20-7 Xylene (total) SU 71-55-6 1,1,1-Trichtoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11UJ 75-27-4 Uromodichloromethane 5U 78-87-5 1,2-Dichtoropropane 5U 10061-01-S cis-1,3-Dichloropropene 5U 79-01-6 Trichloroethene 5U 124-48-1 Dibromochloromethane 51)( 4 Data Reporting Qualifiers: U - compound was analyzed for but not detected. The ntumber is the attainable detection limit for the sample. 8* Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-73
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