C - Hanford Site

WHC-SD-EN-TI-136, Rev. 0
Oak Ridge K-25 Site
Analytical Chemistry Department
BRA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS
TENTATIVELY IDENTIFIED COMPUNDS
AnaLIS ID: 901206-030 Customer Sample ID: N-110
Laboratory: Organic Mass Spectroscopy Laborotor Customer: J. KESSNER/R. SHUCK
Sample Matrix: SOIL File IDN 10659
Level: Clow/med): LOW Date Received: 6-DEC-1990
Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990
% Moisture: not dec. 7.4 dec. _____Date Extracted: 12-DEC-1990
Extraction: (SepFICont/Sonc) SoxH PH: -
GPC Cleanup: (Y/N) N
Concentration Units
Number TIC& found: 12 CugIL or uglKg): gxLK
CAS NUMBER COMPOUND NAME RT IEST. CONC. I 0
I1.
I2.
141-79-71 3-Penten-2-one, 4-methyl-
123-42-21 2-Pentanone. 4-hydroxy-4-methy
4.92 I49"
-b..O "
1 JIA
I3. 872-50-41 2-Pyrrolidinone. 1-methyt-
I4. IUnknown (sat'd Hydrocarbon)
I5. IUnknown (sat'd Hydrocarbon)
I6. IUnknown (Hydrocarbon)
I7. IUnknown (sat'd Hydrocarbon)j
I8. IUnknown 1
I9. jUnknown (Hydrocarbon)
110. jUnknown (Hydrocarbon) 1
I 1.jUnknown (Hydrocarbon) I
9 .E:I'6 2
19.43 I660 J
256 86 j0-
25.89 I850 IJ
u.I
27.671 1500 1
pe.i[ I .490-+. .n
30.531 410j 1
32.60 1420 J .
/
6
12. JUnknown (Hydrocarbon) I 33.45 I 1300I I
113. _ __ _1III
I14.__ _ _ _ j II
I15.__ _ _ _ j II
116. ____
117. 1___
118. ____
119. ____
120.j II
121.11____1
122. 11____1____1___
123.1____1____1 I
24. 1____1____1___
125. I1____1____I___
126. 1_ _ _ _. _ _ _ 1__ _ I
127. II____I____I___
128. - I____ ____I___
129. _____I____i___I
130. I
Data Reporting Qualifiers:
U - Compound was analyzed for but not detected. The nu~mber Is the attainable detection limit for the samp~le.
8 - Anolyte was found in the reagent blank as well as the sample.
j - Indicates an estimated value.
RD - Not detected.
A - Aldol condensation product.
D - Secondary dilution.
E - Exceeds Initial calibration range.
P - Probable Identification. D-51