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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 1 AnaLIS ID: 901206-028 Customer Sample ID: N-108 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. LESSNER/R. SHUCK File ID: 07612 Sample Matrix: SOIL InstrumIent ID: 597012 Reqisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VGA - Volatile Organic Compounds (CL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Nmbier: PURGE & TRAP Analysis Procedure Number: VOA (CLP) NDP Percent Moisture: 5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: CL HUDDLES70N Associated Blank: 901211-004 QA File Number: NA [I : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .................................. .......... ........... .............................. .......... 74-87-3 Chloromethane 11U 79-DO-5 1,1.2-Trlchtoroethane Su 74-83-9 Bromomethane 11U 71-43-2 Benzene SU 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1.3-Dichtoropropene SU 75-00-3 Chtoroethane 11U 75-25-2 Bromoform 5U 75-09-2 MethyLene Chloride % --d L4 108-10-1 4-gethyt-2-pentanone 11U 67-64-1 Acetone 14 LA 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disutfide SU 127-18-4 Tetrachtoroethene, 5U 75-35-4 1,1-Dichloroethene 5U 79-34-5 1,1,2,2-Tetrachtoroethane 5U 75-34-3 1,1-Dichtoroethane SU 108-88-3 Toluene 5U 540-59-0 1,2-Dfchtoroethent (total) 5U 108-90-7 ChLorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1.2-Dichtoroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xytene (total) 5U 71-55-6 1,1,1-Trichtoroethane 5U 56-23-S Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichioromethane 5U 78-87-5 1,2-Dichtoropropane 5U 10061-01-5 cis-1,3-Dichloropropene 5U 79-01-6 TrichLoroethene 5U 124-48-1 Dibromochtoromethane 5U Data Reporting Qualifiers: U - Com~pound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. O - Secondary dilution. E - Exceeds initial calibration range. D-44
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 2 AnaLIS 10: 901206-029 Customer Sample ID: M-109 Laboratory: organic Mass Spectroscopy Laboratory Customer: J9. KESSNER/R. SHUCK Fite I0: 10658 Samrple Matrix: SOIL Instrument ID: 597013 Requisition Number: Authorized Bly: D. C. Canada Date Sample Received: 6-DEC-1990 INA -Base/Neutral/Acid Compoun~ds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Number: Analysis Procedure Number: BNA CCLP) NOP Percent Moisture: 8.0 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEENAN Associated Stank: 901213-028 CA File Number: NA C]:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 108-95-2 Phenol 980U 106-47-8 4-ChLorosnitine 980U 111-44-4 bis(2-Chloroethyl)ether 980U 87-68-3 HexachLorobutadiene 98OU 95-57-8 2-Chlorophenol 980U 59-50-7 4-Chloro-3-methytphenot 9BOU 541-73-1 1,3-Dichtorobenzene 98OU 91-57-6 2-Methytnaphthalene 980U 106-46-7 1.4-Dichtorobenzene 980U 77-47-4 Hexachlorocyclopentadiene 980U 100-51-6 *enzyl Alcohol 98OU 88-06-2 2.4.6-Trichiorophenot 980U 95-50-1 1,2-Dichlorobeniene 9B0U 95-95-4 2.,5-TrichtorophenoL 4700u 95-48-7 2-MethyLphenol 98OU 91-58-7 2-ChLoronaphthalene 980U 108-60-1 bisC2-Chtoroisopropyl)ether 980U 88-74-4 2-Nitroanitlne 470OU 106-44-5 4-Methylphenol 980U 131-11-3 Diuicthylphthalate 980U 621-64-7 N-Nitroso-di-n-propylamine 9B0U 208-96-8 Acenaphthylene 980U 67-72-1 Hexachloroethane 9BOU 99-09-2 3-Nitroanillne 470OU 98-95-3 Nitrobenzene 980tU 83-32-9 Acenaphthene 980Ui 78-59-1 Isophorone 98OU 51-28-5 2,4-Dinitrophenol 4700u 88-75-5 2-Nitrophenol 9B0U 100-02-7 4-Nitrophenot 470OU 105-67-9 2,4-Dimethylphenot 980U 132-64-9 Dibenzofuran 98%. 65-85-0 Benzoic Acid 4)80 .2 d8 LA 121-14-2 2,I.-Dinitrotoluene 98OU 111-91-1 bis(2-Chloroethoxy)methane 980U 606-20-2 2,6-Dinitrotoluene 980U 120-83-2 2,I-DichlorophenoL 980U 84-66-2 Diethytplithalate 4q8 W9-* IA 120-82-1 1,2.4-Trichiorobenzene 980U 7005-72-3 4-Chtorophenyl-phenylether 980U. 91-20-3 Naphthalene 98OU 86-73-7 Fluorene 980U Data Reporting Qualifiers: 4 U - Compound was analyzed for but not detected. The numrber is the attainable detection limit for the samrple. B - Analyte was found in the reagent blank as well as the smple. J9 - Indicates an estimated value. NO - Not detected. A l-Adol condensation product. O - Secondary dilution./ E-Exceeds initial calibration range. Z 1 D-45 4
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P.O. Box 1970 Rfichland. WA 99352 W
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