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WtIC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BHA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-024 Customer Sample ID: N-106 Laboratory: Organic Mass Spectroscopy Laboratoy Customer: J9. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: 10653 Level: (low/med): LOW Date Received: 6-DEC-1990 Dilution Factor: 2.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. 3.3 dec. _____Date Extracted: 12-DEC-1990 Extraction: CSepFICont/Sonc) SoxH PH: GPC Cleanup: (YIN) N Number TiCs found: 9 Concentration Units CugIL or ug/Kg): uqLK. CAS NUM'BER COMPOUND NAME RT EST. CONC. 0 1. 123-42-21 2-Pentanone, 4-hydroxy-4-methy j I : -4v j i ~ 2. 1 Unknown (Atkyt Hydrocarbon) j 19.48 I990 1 1 I3. I4. I5. IUnknown IUnknown (Alkyl Hydrocarbon) 849-99-01 mexanedioic acid, dicyctohexyt 22.031 25.6i 26.39 1 12001.J 1190 4a, 8100 I 6. I7. a . I9. 110. _________________ IUnknown (Hydrocarbon) IUnknown (Hydrocarbon) IUnknown (Hydrocarbon) 1 Unknown 1 !6.49 27.76 1 29.59 1 33.96 1 I 'U 2600 J . 1400 I 9 1300 1. 1 1_____1________ I 11. 1__ _ _ _ 1II 112. __ _ I 113. 1 ____ _________I 14.__ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ _I_ _ _ _ _ _ _ _ I I 15. I II 116. ___________________I______________ ~17. I 18. 119. II I I 120. I21. _ 122. _ _ _ I _1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ I 123.j__________________________ 124. 125. 126.j 127.1 128.1 129.1 130.1II I I I I I I I Data Reporting Qualifiers: U - Coffownd was analyzed for but not detected. The number Is the attainable detection limit for the sample. 83 Analyte was founad in the reagent blank as well as the sample. J.- Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D- 38
WF!C-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 1 AnaLIS ID: 901206-024 Customer Sampte ID: N-106 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 07608 Sample Matrix: SOIL Instrument ID: 597082 Requisition Niuber: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VOA - Volatile Organic Compounds (TCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Number: VGA CCLP) NOP Percent Moisture: 3 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL IIJODLESTON Associated Blank: 901211-004 OA File Number: NA El : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .................................. .......... ........... .............................. .......... 74-87-3 Chloromethane IOU 79-00-5 1,1,2-Trichloroethane 5U 74-83-9 Bromomethane lOU 7 1-43-2 Benzene 5U 75-01-4 Vinyl Chloride I OU 10061-02-6 trans-1,3-Dichtoropropene SU 75-00-3 Chloroethane IOU 75-25-2 Bromform 5U 75-09-2 MethyLene Chloride 5 2*- (A 108-10-1 4-MethyL-2-pentanone IOU 67-64-1 Acetone I1W 591-78-6 2-Hexanone IOU 75-15-0 Carbon Disuifide 5U 127-18-4 TetrachLoroethene 5U 75-35-4 1*1-Dichtoroethene 5U 79-34-5 1*1 92.2-Tetrachloroethane 5U 75-34-3 1,1-Dichloroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Oichtoroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichtoroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone I1W 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-TrichLoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate IOU 75-27-4 Bromodichloromethene 5U 78-87-5 1,2-Dichloropropane SU 10061-01-5 cis-1,3-Dichioropropene 5U L 79-01-6 TrichLoroethene 5U 124-48-1 Dibromochtoromethane 5U Data Reporting Qualifiers: U - Compound was analyzed for but niot detected. The number is the attainable detection limit for the sample. 8 - AnaLyte was found in the reagent blank as well as the sample. J- Indicates an estimated value. RD - Not detected. A - Aldol condensation product. 0 - Secondary dilution. E - Exceeds initial calibration range. D-39
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