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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS 1D: 901206-049 Customer Sample ID: N-126 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File 1D: 3,14511 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BNA - Base/Neutral/Acid Compounjrds CTCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 17JA(19/ Preparation Procedure Numiber: Analysis Procedure Number: SNA C(e,.D Percent Moisture: 8.3 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 QA File Number: NA (I : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ...... ........................... .......... ........... .............................. .......... 108-95-2 Phenol 110007 106-47-8 4-Chloroanitine 11000 7 111-44-4 bis(2-Chloroethyl)ether 11000 7 87-68-3 Nexachtorobutadiene 11000U7 95.57-8 2-Chtorophenot 11000.7 59-50-7 4-Chloro-3-methylphenot 1100071 541-73-1 1,3-Dichlorobenzene 11000.7 91-57-6 2-MethyLnophthaLene i0ou J 106-46-7 1,4-Oichlorobenzene 110oo)07 77-47-4 Nexachtorocyclopentadiene 11000 7 100-51-6 Benzyl Alcohol 11000 7 88-06-2 2,4,6-Trichlorophenot 1100U o 95-50-1 1,2-Dichlorobenzene 110007 95-95-4 2,4,5-Trichlorophenot 5200U07 95.45.7 2-MethytphenoL 1100U7T 91-58-7 2-Chloronaphthatene 110007T 108-60-1 bis(2-Chlorolsopropyt)ether 1100UJ3- 88-74-4 2-NitroaniLine 5200.3 106-44-5 4-MethylpienoL 621-64-7 N-Nitroso-di-n-propyanine 110007 11001.13 131-11-3 DimethyLphthaLate 208-96-8 Acenaphthylene 1100o)03 11000 7 67-72-1 98-95-3 Hexachioroethane Nitrobenzene 11000 7 110007 99-09-2 3-Nitroaniline 83-32-9 Acenaphthene 52000 JT 11000 3' 78-59-1 Isophorone 11000 7 51-25-5 2,4-Dinitrophenol 5200U 7 88-75-5 2-Nitrophenol 1100U7, 100-02-7 4-Nitrophenot 5200U07 105-67-9 2,4-Dimethylphenol 11000,7 132-64-9 Dibenzofuran l11000X 65-55-0 Benzoic Acid 5200U-T 121-14-2 2.4-Dinitrotoluene 1100U.7 111-91-1 bis(2-ChLoroethoxy)methane 110007 606-20-2 2,6-Dinitrotoiuene 11000 T 120-83-2 2,4-Dichlorophenol 10007J 84-66-2 Diethylphthalate 11000 7 120-82-1 1,2,4-Trichlorobenzene 11000 7 7005-72-3 4-Chtorophenyl-phenytether 1100U,7 91-20-3 Naphthalene 110007 : 86-73-7 Fluorene 11000 7 Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The Kx. er is the attainable detection Limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-118 %1
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department 8NA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-049 Customer Sample ID: N-126 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: 2-14511 Level: (Low/med): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 17-JAN-1990 % Moisture: not dec. 8.3 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepFlContlSonc) SoxH pH: ____ CPC cleanup: (YIN) N Concentration Units Num~ber TICs found: 20 (ugIL or ug/Kg): u2L2 CAS NUMBER COMPOUND NAME RT EST. CONC. 0 an:~~ nu:V~zz=2 n~arsf :n:. n m~ 1 ... .... .Z I1. 123-42-21 2-Pentanone, 4-hydroxy-4-methy S.P IA- 440 A IlO 2. 1UNKNOWN HYDROCARBON I 14.13 I 7800 1 3. IUNKNOWN HYDROCARBON I 16.02 I 13000 1 4. IUNKNOWN HYDROCARBON 1 469 4 .43" do 6. _ UNKNOWN HYRCRO 17.781 100 J 6 . I7. IUNKNOWN HDOABNI IUNKNOWN HYDROCARBON I 18.54 18.79 I 10001 5800 J a. IUNKNOWN HYDROCARBON I 19.41 1 6000 J I9. IUNKNOWN 19I.R0 ROOI.. d 1 1. IUNKNOWN HYDROCARBON I 20.38 1 4200 J 1 11. IUNKNOWN HYDROCARBON I 20.97 I 15000 J 12. 13. IUNKNOWN HYDROCARBON IUNKNOWN HYDROCARBON I I 21.67 I 22.43 I 8400 16000 1 1 14. UNKNOWN HYDROCARBON I 22.52 I 8400 J 15. UNKNOWN HYDROCARBON HIB We de-I." 16. UNKNOWN HYDROCARBON I 23.93 I 7300 J 17. 18. 19. UNKNOWN HYDROCARBON UNKNOWN ARAMATIC KETONE [UNKNOWN HYDROCARBON 25.4 260 I 26 238 ; 0C0 le-O 9"&c I I3' I 20. jUNKNOWN HYDROCARBON Z7.4 5; *0 -asoI 121.______ I 122.__ _ _ _ II I 123. _ _ _ _ 1IIII 124. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ _I_ _ _ _ _I_ _ _ 25. 1__________________1______ ______1____ 126. _ _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ _ _ _ _1_ _ _ 127. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _1_ _ _ _ _1_ _ _ 128.1__ _ _ _1_ _ _ _ 1__ _ I 129. __ _ _ _I_ _ _ _ i__ _ I 130.1__ _ _ _1_ _ _ _ 1__ _ Data Reporting Qualifiers: U - Compoun~d was analyzed for but not detected. The number is the attainable detection limit for the sample. B -Analyte was found in the reagent blank as well as the sample. J4 Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D0 Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D-119 ~
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