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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS I0: 901206-044 Customer Sample 10: N-122 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: ),14473 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 5-DEC-1990 INA - Base/Neutral/Acid Compounids (TCL) Date Extracted/Prepared: 13-DEC- 1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Numb~er: Analysis Procedure Number: SNA (CIP) HOP Percent Moisture: 5.9 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 CA File Number: NA 11 : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .................................. .......... ........... .............................. .......... 100-01-6 4-Nitroaniline R 480OU 53-70-3 Oibenz(a,h)anthracene R 99OU 534-52-1 4,6-Dlnitro-2-methylphenot R 4800U 191-24-2 Benzo(g,h,i)perylene R 990U 86-30-6 N-Nitrosodiphenylamine R 990U 101-55-3 4-Bromophenyl-phenylether R 990U 118-74-1 Hexachlorobenzene R 990U 87-86-5 Pentachlorophenot R 4800U 85-01-8 Phenanthrene R 990U 120-12-7 Anthracene R 990U. 84-74-2 Di-n-butylphthalate 7100S..LA, 206-44-0 FLuoranthene R 990U 129-00-0 Pyrene R 990U 85-68-7 ButylbenzyLphthalate R 990U 91-94-1 3,3'-DichLorobenzidine R 2000U 56-55-3 Benzo(a)anthracene R 990U 117-81-7 bis(2-EthylhexyL)phthatate R 990U 218-01-9 Chrysene R 990U 117-84-0 Di-n-octylphthalate R 990U 205-99-2 Benzo(b)fluoranthene R 990U 207-08-9 genzo(k)ftuoranthene R 990U 50-32-8 Benzo(a)pyrene R 990U7/ . 193-39-5 Indeno(1,2,3-cd)pyrene R 990U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number Is the attainable detection limit for the sample. B - Analyte was found In the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Atlol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-102
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department DNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS 1D: 901206-044. Customer Sample ID: N-122 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: >14473 Level: (towlmed): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. 5.9 dec. _____Date Extracted: 13-DEC-1990 Extraction: CSepFlContlSonc) SoxH PH: ____ CPC Cleanup: (YIN) N Concentration Units Number TICs found: 20 (ugIL or ug/Kg): _uK I CAS NUMBER COMPOUND NAME RT jEST. CONC. 0 I1. 123-42-21 2-Pentanone. 4-hydroxy-4-methy J5.r69- ;9000 1 dAe0 I2. _ jUNKNOWN 1 j8.28j 650 1 1 I3. 1 UNKNOWN ALCOHOL 3 -~99m-4- H00-4,1 I4. _____ jUNKNOWN ACID 15.61 I46011 I5. jUNKNOWN -.9 4OI9094 d o 6. ___ jUNKNOWN ZO79 7. _______jUNKNOWN 1T! 20 d o, 8.______ UNKNOWN j 1.90I ~ 00 I9. jUNKNOWN PNTHALATE ESTER 266 iio -I e I10. UNKNOWN HYDROCARBON J 24.83 I3400 1 1 11. jUNKNOWN HYDROCARBON ~I70IJ I12. ______jANTHRACENEDIONE oi.I 7QI9 13. jUNKNOWN HYDROCARBON 2J3 9; I~ N; 14. 15. IUNKNOWN HYDROCARBON f UNKNOWN HYDROCARBON J V-1 .? I 2?0 N100 d7o -I.i i a; /16. IUNKNOWN ; 9.6; go 00 0 17. I18. IUNKNOWN HYDROCARBON IUNKNOWN HYDROCARBON 29.84 500 -------- '; 2408O J 19. I20. jUNKNOWN HYDROCARBON UNKNOWN HYDROCARBON 31 70 I ------ 4904-s - 1 999 j0 121. ____11 I 122.11 I 123.__ _ _ 11 I /24. 1 I /25. ____ 126.1 II 127.1 I 128.1I I 129. I 130.j II Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numb~er is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the saawple. J - Indicates an estimated value. RD -Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D-103 .
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