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WIlC-SD-EI-TI-136, Rev. ')<br />

Oak Ridge K-25 <strong>Site</strong><br />

Anal ytical Chemistry Department<br />

INA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS<br />

TENTATIVELY IDENTIFIED COMPOUNDS<br />

AnaLIS ID: 901206-046 Customer Sample 10: N-124<br />

Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK<br />

Sample Matrix: SOIL Fite ID: ),14475<br />

Level: (low/med): LOW Date Received: 5-DEC-1990<br />

Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991<br />

% Moisture: not dec. 7.1 dec. _____Date Extracted: 13-DEC-1990<br />

Extraction: (SepF/Cont/Sonc) SoxH pH: ____<br />

GPC Cleanup: (Y/N) N<br />

Concentration Units<br />

Nuber TICs found: 20 Cug/L or uglKg): u2LK2<br />

CAS NUMBER COMPOUND NME RT IEST. CONC. a<br />

~ O ~<br />

1.<br />

I2.<br />

I3.<br />

I4.<br />

123-42-21 2-Pentanone. 4-hydroxy-4-methy<br />

1 UNKNONW ALCOHOL<br />

1 UNKNOWN ALCOHOL<br />

1 UNKNOWN<br />

6.! I<br />

Q18<br />

+6i; 2<br />

"A-u<br />

66 8J<br />

~ 3000 in~ -<br />

Me H3~<br />

I5.<br />

I6.<br />

I7.<br />

8.<br />

1 UNKNOWN<br />

1 UNKNOWN<br />

1 UNKNOWN<br />

1 UNKNOWN HYDROCARBON ~<br />

1?.ee I 10I.I<br />

19,10I 7OOI ~<br />

288 Z500 4-46-~<br />

M .oIS 658oI<br />

9. [UNKNOWN PHTHALATE ESTER N .6?. 1.<br />

I10. IUNKNOWN HYDROCARBON I 24.84 I1500I<br />

11. IUNKNOWN HYDROCARBON 22.090<br />

I12. IANTHRACECOIONE 28e i 1OOis .D<br />

13. [UNKNOWN HYDROCARBON ?63 8 0I.<br />

14. [UNKNOWN HYDROCARBON N9T.66 1 leg d .<br />

15. UNKNOWN HYDROCARBON ?0Z.;c4 XCOG.I '<br />

16. ______jUNKNOWN ALKOXY COMPOUND I cy.se F 0 IJ<br />

I17. jUNKNOWN HYDROCARBON 1 29.80 1 2100 j.<br />

18. UNKNOWN HYDROCARBON i n RA iOj4.<br />

19. UNKNOWN HYDROCARBON 34~.68 6;90o~<br />

20. jUNKNOWN ALKOXY COMPOUND j 37.26 j1200 j 1<br />

121.1__ _ _ _ _ _ _ _ _ _ j__ _ _ __ _ _ I__ _<br />

122.111__ _ _ 1__ _<br />

123.1__ _ _ _ _ _ _ _ _ _ __ _ _ 1__ _ _ 1__ _<br />

124. I<br />

125. II<br />

126. I I<br />

127. II<br />

128. I<br />

129.I I<br />

130. II<br />

Data Reporting Qualifiers:<br />

U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample.<br />

B - Analyte was found in the reagent blank as well as the sample.<br />

J Indicates an estimated value.<br />

RD -Not detected.<br />

A - AldoL condensation product.<br />

D - Secondary dilution.<br />

E - Exceeds initial calibration range.<br />

P-Probable identification. D-111

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