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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge Ir-25 <strong>Site</strong> 50 Analytical Chemistry Department Results .t Analyses AmmS 10, 90122"507 Proe.cti 0132 027S Customer Sample 10: 2710a Cotmar, inS~o5kk Requisition Nmbe: Date Sampled: 18-M~-1990 Dte Sample Received: 20-MU-1990 Sampld 3 1 c: Dote Sample Copleted: 27-JAMI-l991 material Description: SOIL (I:Result has beam Corrected for Spike ACtiv. GA Date Nmber Procedure no. Analysis Result units Analyst Fie u.mber COWletod 102003 ZPA-3050 Load 4.3 Usyg P SUCZZ 16123R 27-Jam-1991 PAF-7421 132803 SPA-3550 Prep 131%- S*446-Sexy C in ShIS 1"93 4-JAM-1991 Prep (XHA- SW-846-Sou) Analyst - 33S SRI= Date Extracted - 3-JAII-1991 Sample IWight gxtracted (q) a 10.60 Percent Solids - 92.5 Calculated Dried Weight 1g) a 9.81 Etraction Method a Sshlet Extraction solvent - Hathlylen. ailoud/Acetone Etraction Cleanup a Sodium Sulfate Final Volume of Extract (maid I Associated Blank - 910103-263 *** Comments from the Ocganic mass Spectroseopy Laboratory TZuu SAMPLE wC NOT NUET CLI W Olt LABSAIMR GAP M1!UI FOR SURMOGATE STANDARD % ROERY FOR ZZIAUBL NAMau. TWO OR IC SUINCOWS STwAMIRS WZR OUysXD APTwANCE CRIIRA, wuuXT WA TO URX ZmFCT AND DUmAITm. ZUUSA STAM MODAWS N wnumZ CLP SOW AM LKNOAM GW D-212 Program Manager: 0. L. Amburgey Date Approved: 7-rED-1991
WHC-SD-EN-TI-136, Rev. 0 AnLtS DsAOTA US~Pag, ADaLIS to: 90122"-57 Customer Sample Io: 27-105 -Laboratory: Organic Mans Spectroscopy Laboratory customer: X9S8HiNO00 rile IV: 10935 Sape Matrix: SOIL Insumnt IV. 5970--3 Requiition nmber: Authorized by: 0. C. Canada oate Sample Received: 20-MU-1990 SEA - D sefU~tral/Acid Compounds (TC.3 Dats xxtracted/Prepared: 3-JMI-1991 onto Analysed, 14-JAS-1991 Preparation Procedure nmers ZPA-3330 Analysis Procedure Suabt: Ift ( HL) OP percent Moisture: 7.5 Dilution Factor: 5.0 percent moisture (decanted): Analyst: C IIM Associated Blank: 910103-263 1%W rile amber: Wh ti Result bas beom corrected for Spike 1 of 2 ChM mg/Kg CS m/I; 10$-95-2 Phenol SOOOU 106-47-8 4-Welroanilile 500 111-44-4 blat 2-diloroethyl )ether 50001U 67-48-3 llezachlorobutadiene 500OU 95-57-8 2-Chlorepbenol, 500013 59-50-7 4-Chloro-3-mothylphsIol 10001 541-73-1 1, 3-Dichlorobeflsefe 500013 91-S7-6 2-mathyluaghthalefte 35000 10"-6-7 1, 4-Dichloraoenan 500013 77-47-4 Ilexachl orocyclopefltadiefle 50001 10"-1-4 Deesyl, Alcohol 5000u3 86-04-2 2,*4 ,6-fTichorophelldl 500013 95-50-1 1, 2-Dichlorobeuisene 500013 9"-5-4 2,4.3 -frichloraph -,I 2400013 95-40-7 2-Naothylphenol 500013 91-5W7 2- W oronapbthaleno 50001 10"-0-1 biat 2-chloroiapopyl ether 5001 88-74-4 2-ftroaniline 2400013 106-44-5 4-Nothylpbeol 50001 131-11-3 Dimsthylpbthalate 5001 621-44-7 N-Mit roso-di-n-propylamile 500013 208-96-8 Acenahthylene 50001 67-72-1 Hexachloroethane 500013 99-09-2 3-alit roamiline 2400013 98-5-3 Nitrobeasene 500013 83-32-9 Acenaphthete, 2000 .7 7"-9-1 Isoghorone 500013 51-20m-5 2,4-Dinitopheflal 2400013 88-75-5 2-fitrophmW 500013 100-02-7 4-Nitrephenol 240003 105-67-9 2 ,4-Dimethylpbenol 500013 132-4- Diheasofuran 500013 45-85-0 Sensoic Acid 2400013 121-14-2 2,*4-Diaitrotoluene 50001U 111-91-1 bist 2-Chloroethoxy methane 500013 606-20-2 2 .6-Olnitrotoluefl 500013 120-$3-2 2, 4..Dchboropbemol 500013 84-46-2 Diethylphthalate 500013 120-82-1 1,2 ,4-Trichlorobnuefle 50001 7005-72-3 4-Wuoropheay1-ghenwlether 508013 9 1-20-3 naphthalene 500013 86-73-7 Fluorene 940 J7 Data Reporting Qualifiers: 13 - Comouond wasn analyzed for but not detected. The number is the attainable detection limit for the sample. a - Analyte was found in the reagent blank as well anthe sample. J7 - Indicates an estimated value. RD - not detected. A - Aldol condensation product. 0 - Secondary dilution. 9 - Exceeds initial calibration rang. D-213
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Dae Reced INFORMATION RELEASE REQUE
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INTRODUCTION WC-SD-EN-TI-136, Rev.
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P.O. Box 1970 Rfichland. WA 99352 W
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Analysis A. Semi-Volatiles B. Volat
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