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WIIC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLlS ID: 901206-036 Customer Sample ID: N-116 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: )14465 Level: (lowlmed): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. - 6.3 dec. Date Extracted: 13-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxH PH: GPC Cleanup: (TIN) N Concentration Units Numb~er TICs found: 18 (ugIL or uglKg): u K CAS NUMBER ICOMPOUND NAME RT IEST. CONC. a ~ 222222322222222222222Z222:3222 222222222: j 2222232222223 I322222222 I1. 123-42-21 2-Pentanone. 4-hydroxy-4-methy j.6 "'QQl 3 1 .A:1 2. I3. 4. I5. I6. I7. I8. I9. I10. 1 UNKNOWN jUNKNOWN ALCOHOL jUNKNOWN ALCOHOL jUNKNOWN UNKNOWN j.UNKNOWN HYrDROCARBON UNKNOWN HYDROCARBON jUNKNOWN PHTHALATE ESTER jUNKNOWN j 6.061 J.36 I 1).00I 1F.48L~ 2 O.94 23Mi~uI R.9 j 1. 0 I 1 24.841 420 1j 6to do~ Ju~ IJ 8900 o 1 IJ We 01J 8401 .1 I11. UNKNOWN HYDRICARUON s.1ig goo~e 12. 13. UNKNOWN HYDROCARBON jUNKNOWN HYDROCARBON j 2 6. 5OI 6 27.5n I 1fpl 10 14 UNKNOWN HYDROCARBON j80 o~Iad~r 15. UNKNOWN HYDROCARBON 298 I me . a50I 16. UNKNOWN HYDROCARBON 401!? 1 ! 220 I 17. jUNKNOWN ALKOXY COMPOUJND j 1 .i 18. UNKNOWN HYDROCARBON 31.3 I (0i .e 119. 120.1__ 121. 1_ _ _ _ _ _ _ _ _ _ _ _ _ 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 1__ _ _ _ _ _ _ _ 1__ _ _ _1_ _ _ _ _ _ _ __ _ _ _ _ I 122. 123.1__ 124.1__ 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ 1__ _ _ 1__ _ _ _ _ _ _1_ _ _ _ 1__ _ _1_ _ _ 1__ _ _ 1__ _ I 25.__ _ _ _ _ _ _ _ _ _ 1__ _ _ _1_ _ _ _ 1__ _ 126.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ 1__ _ _ 1__ _ 127.1 I I 128.I I 129. I 130. I Data Reporting Qualifiers: U - Compound wos analyzed for but not detected. The numb~er Is the attainable detection limit for the sample. B - Analyte wias found in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO -Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P-Probable identification. D-76
WHIC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 1 nLIS ID: 901206-036 Customer Samle ID: N-116 Laboratory: Organic 1Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07586 Sample Matrix: SOIL Instrument ID: 597002 Requisition Number: Authorized By: D. C. Canada Date Sampte Received: 5-DEC-IM9 VDA -Volatile organic Compounds (TCI.) Date Extracted/Prepared: Date Analyzed: 10-DEC- 1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Nuumber: VOA (CLP) NOP Percent Moisture: 6 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: SL STAFFORD Associated Blank: 901210-025 CA File Number: NA U:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 74-87-3 Chloromethane 11U 79-00-5 1.2-Trichtoroethane SU 71.-83-9 Bromomethane 11U 71-43-2 Benzene SU 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichloropropene 5U 75-00-3 Chloroethane 11U 75-25-2 Breonoform SU 75-09-2 Methylene Chloride 3 d-9' LA, 108-10-1 4-Methyl-2-pentanone 11U 67-64-1 Acetone 11u 591-75-6 2-Hexanone 11u 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachloroethene 5U 75-35-4 1,1-Dichloroethene SU 79-34-5 1,1,2,2-Tetrachioroethane 5U 75-34-3 1,1-Dichtoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichtoroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichloroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1.1-Trichtoroethane 5U 56-23-S Carbon Tetrachloride 5U 108-05-4 Vinyl. Acetate 11U 75-27-4 Bromodichloromethane SU 78-87-5 1,2-Dichloropropane 5U 10061-01-5 cis-1.3-Dichloropropene 5U 79-01-6 Trichioroethene 5U 124-48-1 Dibromochloromethane 5U CotmRpoutn Qaualyziedrosu:o eece. Tent~r steatial Dat Repotng waualies: o dtce.Te ubri heatial detection limit for the sample. B Analyte was found in the reagent blank as well as the sample. J -Indicates an estimated value. RD -Not detected. A -Aldol condensation product. D -Secondary dilution. E -Exceeds initial calibration range. D-77
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P.O. Box 1970 Rfichland. WA 99352 W
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