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u;IC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT *Page 2 of 2 AnaLiS ID: 901206-047 Customer Sample ID: N-125 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: )14476 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Numb*er: Authorized By: 0. C. Canada Date Sample Received: 5-DEC-1990 BNA - Base/Neutral/Acid Compounds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAN- 1991 Preparation Procedure Number: Analysis Procedure Number: SNA (CIP) NDP Percent Moisture: 6.5 Dilution Factor: 1.0 Percent moisture (decanted): Analyst: AK HEADRICK Associated Btank: 901214-083 GA File Number: NA 11 : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .................................. .......... ........... .............................. .......... 100-01-6 4-Nitroaniline Rt 5 100U 53-70-3 Dibenz~a~h)anthracene R 1000u 534-52-1 4,6-Dinitra-2-methytphenot R 5100U 191-24-2 Uenzo(g,h,i)perylene R 1000U 86-30-6 N-Nitrosodiphenylamine R 1000tJ 101-55-3 4-Bromopheny-phenylether R 100OU 118-74-1 Hexachlorobenzene R 1000U 87-86-5 Pentachlorophenol R 5100U 85-01-8 Phenanthrene 2200 120-12-7 Anthracene R 1000U 84-74-2 Di-n-butylphthaLate 5 6 00 11,u 206-44-0 Fluoranthene R IOOOU 129-00-0 Pyrene R IOOOU 85-68-7 ButytbenzylphthaLate R 1001. 91-94-1 3,3'-DichLorobenzidinte R 2101U 56-55-3 Benzo(a)anthracene R 1000U 117-81-7 bis(2-Ethythexyt)phthalate R 1000U 218-01-9 Chrysene R 1001. 117-84-0 Di-n-octylphthalate R 1000U 205-99-2 Uenzo(b)ftuoranthene R 1000U 207-08-9 Denzo(k)fLuoranthene R 1000U 50-32-8 Benzo(a)pyrene R 10011 193-39-5 Indeno(1,2,3-cd)pyrene R 1000U Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The numiber is the attainable detection limit for the sample. B Analyte was found in the reagent blank as well as the sample. J -Indicates an estimated value. NDO Not detected. A -Aldol condensation product. D -Secondary dilution. E -Exceeds initial calibration range. D-1214
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department DNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-047 Customer Sam~ple iD: N-125 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J9. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: ),14476 Level: (Low/med): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. 6.5 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepFlContlSonc) SoxH pH: ____ GPC Cleanup: (YIN) N Number TICs fo und: 20 Concentration Units (ugIL or uglKg): ug/K2 CAS NUMBER COMPOUND NAME FIT EST. CONC. a 1 . 123-42-21 2-Pentanone, 4-hydroxy-4-methy I 5.7 it ftsee I2. 1 UNKNOWN HYDROCARBON j 14.12 I 12000 I~ I3. .jUNKNOWN HYDROCARBON j 16.03 I 23000 I. I4. 1UNKNOWN HYDROCARBON J 17.3e Fees .~ I5. jUNKNOWN HYDROCARBON j 17.81 I 22000 J I I6. jUNKNOWN HYDROCARBON j 18.56 I8500 I. I7. jUNKNOWN HYDROCARBON j 18.82 12000 J. I8. I9. UNKNOWN HYDROCARBON [UNKNOWN j 1 19.46 I 19.741 28000 1 9 22000 1I 10. I11. I12. I13. jUNKNOWN HYDROCARBON 1UNKNOWN UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON j j j 20.41 I8200 . 1 2 0.94 I 1eee" Ido 20.98 j 17000 . 1 21.70 j 25000 1 . 14. 15. UNKNOWN HYDROCARBON jUNKNOWN HYDROCARBON j J 22.46 j 22.55 l 42000 23000 1 . 1 9 16. IUNKNOWN HYDROCARBON ; 1.s4 4- 34e00 1 do 17. 18. IUNKNOWN HYDROCARBON IUNKNOWN HYDROCARBON I 23.96 1 18000 1 .9 2 - 1 &-4------VT_-t-1j .9 19. IUNKNOWN HYDROCARBON 26.I40 1 2C;0 i. 20. IUNKNOWN HYDROCARBON I" 2768seC3I 121. III.._ _ _ 122.II ___I 123. III. _ _ j24. ___I 125.I I__ _ 126.I ___I 127. II___I 28. ___I 129.I I ___I 130. II. __ Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number Is the attainable detection limit for the samp'le. B - Analyte was found in the reagent blank as well as the sample. J.- Indicates an estimated value. ND - Hot detected. A - Aldot condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D-115
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