C - Hanford Site

WHC-SD-EN-TI-136, Rev. 0
Oak Ridge K-25 Site
Analytical Chemistry Department
INA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS
TENTATIVELY IDENTIFIED COMPOUNDS
AnaLIS ID: 901206-045 Customer Sample ID: N-123
Laboratory: Organic Mass Spectroscop~y Laboratory Customer: J. KESSNER/R. SHUCK
Sample Matrix: SOIL File ID: 3,14474
Level: (low/mad): LOW Date Received: 5-DEC-1990
Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991
% Moisture: not dec. 8.5 dec. _____Date Extracted: 13-DEC-1990
Extraction: CSepF/Cont/Sonc) SoxH PH: ____
GPC Cleanup: (YIN) Nj
Concentration Units
Number TICs founid: 20 Cug/L or ug/Kg): _tsgK2
CAS NUMBER COMPOUND NAME RT EST. CONC.
I1. 123-42-21 2-Pentanone. 4-hydroxy-4-methy
2. 1 UNKNOWN
I3.1 UNKNOWN ALCOHOL
I .65- --- iOfl0 -
15.721 95011 J
438 07 --- I d9 -
I~e
4 .___ _ 1 UNKNOWN 10.90I No"I do
I5.
6.
I7.
jUNKNOWN
JUNKNOWN
jUNKNOWN
I 19.0
i9.?e I40
20!.90 I3e
3neOIJ ! d
I~ d9o
I de
a .
9.
jUNKNOWN HYDROCARBON
1UNKNOWN PHTHALATE ESTER
I 3.7 f I
-?*-~ 60 -~
I11. IUNKNOWN HYDROCARBON I, jt- I
1 2.
I13.
14.
IANTHRACECOTONE
IUNKNOWN HYDROCARBON
IUNKNOWN HYDROCARBON
I65
I
I
j I
Q00
9;
d o
i IM)0
I .
I15. IUNKNOWN HYDROCARBON 2e.7 F9 -"GO Ie-
16. IUNKNOWN ALKOXY COMPOUND j -9.159O
17. IUNKNOWN HYDROCARBON 29.81 I2900 .1
18. IUNKNOWN HYDROCARBON I 3
0.85, C o--o
19.
I20.
UNKNOWN HYDROCARBON
IUNKNOWN HYDROCARBON
I 5l.?V ;8700 I "
nan.7I
121. II___
122. II___
123. IIIJ___
124. J__ _
125. III___
126. III___
127. I __ _ I
28.IIJ__ _
129. IIJ___
130.I I
Data Reporting Qualifiers:
U -Compound was analyzed for but not detected. The numb~er is the attainable detection Limit for the sample.
B8 Analyte was found in the reagent blank as well as the sample.
J Indicates an estimated value.
ND -Not detected.
A Aldol condensation product.
D Secondary dilution.
E -Exceeds initial calibration range.
P -Probable Identification. D-107