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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLS I: 90206021Customer Sample ID: N-103 Laboratory: Organic Kass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 10648 Sample Matrix: SOIL Instruaent 10: 597003 Requisition Numb~er: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BRA - Base/Neutral/Acid Compounds CTCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Number: Analysis Procedure Numbier: BNA (CIP) NOP Percent Moisture: 5.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 GA File Numbrder: NA El : Result has been Corrected for spike CAS Ug/Kg CAS ug/Kg 108-95-2 Phenol 1000U 106-47-8 4-ChtoroaniLine 1000U 111-44-4 bis(2-Chtoroethyt)ether 1000U 87-68-3 Hexachtorobutadiene l0Ou 95-57-8 2-Chlorophenot 1 000U 59-50-7 4-Chloro-3-methytphenot 1000U 541-73-1 1,3-Dichtorobenzene I 000U 91-57-6 2-Methytnaphthatene 100OU 106-46-7 1,4-DichLorobenzene 1OOOU 77-47-4 Nexachtorocyclopentadiene I 000u 100-51-6 Benzyt Alcohol, 1000U 88-06-2 2,4,6-TrichtorophenoL l0OUt 95-50-1 1,2-Dichlorobenzene I 000U 95-95-4 2,4,5-TrichloropheroL 5100u 95-48-7 2-MethyiphenoL 100OU 91-58-7 2-ChLoronaphthatene 1000U 108-60-1 bisC2-Chloroisopropyt)ether 100OU 88-74-4 2-Nltroanitine 510Wu 106-44-5 4-Methylphenot IOO0OU 131-11-3 Dimethylphthalate 1000U 621-64-7 N-Nitroso-di-n-propytamine I 000U 208-96-8 Acenaphthylene 1000U 67-72-1 Hexachtoroethane 1000U 99-09-2 3-NitroaniLine 51OU 98-95-3 Nitrobenzene 1 00WU 83-32-9 Acenaphthene 1000W 78-59-1 Isophorone I100WU 51-28-5 2.4-Dinitrophenol Sl00U 88-75-5 2-Nitrophenol 100WU 100-02-7 4-Mitrophenot 5Ou 105-67-9 2,4-Dimethytphenot IOOOU 132-64-9 Dibenzofuran 1000U 65-85-0 Benzoic Acid 510WU 121-14-2 2,4-DinitrotoLuene 1000u 111-91-1 bis(2-Chloroethoxy)methane 100OW 606-20-2 2,6-Dinitrotoluene 1000U 120-83-2 2,4-Dichlorophenol 100WU 84-66-2 Diethytphthalate 1000 doQ-G ( 120-82-1 1,2,4-Trichtorobenzene 1000U 7005-72-3 4-ChLorophenyl-phenylether 100OW 91-20-3 Naphthalene 100WU 86-73-7 Fluorene l0OU Data Reporting Qualifiers: U - Conpound was analyzed for but not detected. The numaber is the attainable detection limit for the samrple. 8 - Analyte w~as found in the reagent blank as well as the samrple. J - Indicates an estimated value. NO - Not detected. A-Aldol condensation product. O - Secondary dilution. E - Exceeds initial calibration range. D-24
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS 10: 901206-021 Customer Sample ID: N-103 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 10648 Sample Matrix: SOIL instrument ID: 597003 Requisition Numbr: Authorized By: 0. C. Canada Date Sample Received: 6-DEC-1990 BNA - Base/Neutral/Acid Compounds CTCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Nuber: Analysis Procedure Number: DNA (CLP) HOP Percent Moisture: 5.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C KEENAN Associated Blank: 901213-028 QA File Numb~er: NA EU : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ......................... ...... .......... ........... .............................. .......... 100-01-6 4-Nitroaniline 510OU 53-70-3 Dibenz~a,h)anthracene IOOOU 534-52-1 4,6-Dinitro-2-methytphenoL 5100U 191-24-2 Benzo(g,h~i)perylene 1000U 86-30-6 *N-Nitrosodiphenylamine 1000U 101-55-3 4-Iromophenyl-phenylether 1000U 118-74-1 Hexachlorobenzene 100OU 87-86-5 PentachiorophenoL 5100U 85-01-8 Phenanthrene 1000U 120-12-7 Anthracene 100OU 84-74-2 Di-n-buitylphthaLate 2900 S, LA 206-44-0 Fluoranthene 100OU 129-00-0 Pyrene 1000U 85-68-7 Iutytbenzytplhthatate 1000U 91-94-1 3,3'-Dichlorobenzidine 2100U 56-55-3 *enzo~a)anthracene 1000U 117-81-7 bis(2-Ethylhexyl)phthatate 5ie d- too~o LA 218-01-9 Chrysene 1000u 117-84-0 Di-n-octylphthaLate 1000U 205-99-2 *enzo(b)ftuoranthene I 000U 207-08-9 Senzo(k)ftuoranthene 100OU 50-32-8 Benzo(a)pyrene 1000U 193-39-5 Indeno(1,2,3-cd)pyrene IOOOU Data Reporting Qualifiers: U - Compoun~d was analyzed for but not detected. The number is the attainable detection limit for the sample. 8 - Anatyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. q& q D-25
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