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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of I AnaLlS ID: 901206-045 Customer Sample 10: N-123 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File 10: 07595 Sample Matrix: SOIL Instrument ID: 5970#2 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 5-DEC-1990 VOA -Volatie organic Compounds CTCL) Date Extracted/Prepared: Date Analyzed: 10-DEC- 1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Number: VGA CCLP) NDP Percent Moisture: 9 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: SL STAFFORD Associated Blank: 901210-025 GA File Nuber: NA Dl : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 74-87-3 Chtoromethane 11U 79-00-5 1.1,2-Trichloroethane 5U 74-83-9 Broi methane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1.3-Dichtoropropene SU 75-00-3 Chloroethane 11t; 75-25-2 Bromoform 5U 75-09-2 Methytene Chloride -5 2n- LA 108-10-1 1-Methyt-2-pentanone 11U 67-61 Acetone 17- S 1A 591-78-6 2-Ilexanone 1 1U 75-15-0 Carbon Disulfide SU 127-18-4. Tetrachloroethene 5U 75-35-4 1,1-Dichloroethene 5U 79-34-5 1,1.2,2-TetrachLoroethane 5U 75-34-3 1,1-Dichtoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichloroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichloroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xyleme (total) 5U 71-55-6 1,1,1-Trichtoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4. Vinyl Acetate 11U 75-27-4 Bromodichioromethane 5U 1006-01-5 c1,3-Dchorropone 5U 7806-87-5 c1,-Dichloroprne 5U 79-01-6 TiichLoroethene 5U 124-48-1 Dibromochtoromethane 5U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Anslyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-108
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORiT Page 1 of 2 AnaLIS ID: 901206-046 Customer Samiple ID: N-124 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: ),14475 Sample Matrix: SOIL Instrument ID: MP-5985 Requisition Number: Authorized Dy: 0. C. Canada Date Sample Received: 5-DEC-i990 DNA - lase/Meutral/Acid Compounds (TCL) Date Extracted/Prepared: 13-DEC- 1990 Date Analyzed: 2-JAN- 1991 Preparation Procedure Nurter: Analysis Procedure Number: DNA (CLP) HOP Percent Moisture: 7.1 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Stank: 901214-083 CA File Number: NA U:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 108-95-2 Phenol ft 1000W 106-47-8 4-ChtoroaniLine ft 10003 111-44-4 bisC2-Chloroethyt)ether ft 100013 87-68-3 Hexachtorobutadiene R 10013 95-57-8 2-Chlorophenot ft 100013 59-50-7 4-Chloro-3-methylphevot ft 100013 541-73-1 1,3-Dichtorobenzene ft 100013 91-57-6 Z-Methyinaphthalene ft 10001 106-46-7 1,4-Dichlorobenzene ft 1000U 77-47-4 Hexachtorocyclopentadiene ft 10001 100-51-6 Renzyl Alcohol ft 100013 88-06-2 2,4,6-Trichtorophenot ft 10003 95-50-1 1,2-Dichiorobenzene ft 10003 95-95-4 2,4,5-Trichlorophenot ft 480013 95-48-7 2-MethylphenoL ft 100013 91-58-7 2-Chloronaphthatene ft 100013 108-60-1 bis(2-Chloroisopropyt)ether ft 100013 88-74-4 2-Nitroanitine Rt 680013 106-44-5 4-Methylphenol R 100013 131-11-3 Dimethyiphthatate ft 100013 621-64-7 N-Nitroso-di-n-propylamine ft 10003 208-96-8 Acenaphthylene ft 1000U 67-72-1 Hexachloroethane ft 100013 99-09-2 3-NitroaniLine ft 48001U 98-95-3 Nitrobenzene ft 10003 83-32-9 Acenaphthene ft 100013 78-59-1 Isophorone ft 100013 51-28-5 2,4-Dinltrophenot ft 48001U 88-75-5 2-Nitrophenol ft 10001. 100-02-7 4-Nitrophenol ft 480013 105-67-9 2,4-pimethyiphenol ft 100013 132-64-9 Dibenzofuran ft 100013 65-85-0 Benzoic Acid R 480013 121-14-2 2,4-Dinitrotoluene ft 100013 111-91-1 bis(2-Chtoroethoxy)methane ft 100013 606-20-2 2,6-Dinitrotoluene ft 100013 120-83-2 2,4-Dichtorophenol ft 100013 84-66-2 Diethylphthatate ft 10003 120-82-1 1,2,4-Trichlorobenzene ft 100013 7005-72-3 4-Chlorophenyi-phenytether ft 100013 91-20-3 Naphthalene ft 10003 86-73-7 Fluorene R 100013 Data Rteporting Oualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A - Aldot condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-109
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