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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BRA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED C0MI)WNDS AnaLIS ID: 901206-020 Customer Sample ID: N-102 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J1. KESSNER/R. SHUCK Sample Matrix: SOIL Fite ID: 10647 Level: (tow/med): LOWJ Date Received: -6-0EC-1990 Dilution Factor: 1.0 Date Analyzed: 13-0EC-1990 % Moisture: not dec. 7.7 dec. On____Dte Extracted: 12-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxH PH:_____ GPC Cleanup: (YIN) N Concentration Units Numb~er TICs found: 14 (ug/L or uglKg): y~_K CAS NUMBER j COMPOUND NAME RT EST. CONC. Q 1. I2. 123-42-21 2-Pentenone._4-hydroxy-4-methY 872-50-41 2-Pyrrotidinone._1-methyl- I 9-"I~ 9.03 I 30 3. 25013-16-51 Phenot.(1.1-dimethytethyt)-4-m i14;7 I 54" 4. 1 Unknown I 10.08 ia 1303 d I5. 17851-53-51_1.2-Benzenedicarboxytic acld.b 6. IUnknown (sat'd Hydrocarbon) I7. Iunknown 8. IUnknown (sat'd Hydrocarbon) I I j 2.31 --2S.6~1 I 26.001 60- I a 60I .s 4601. 6 I 9. IUnknown J 27.70 I2100 I. 10. IUnknown (Atkyl Hydrocarbon) 26A1 3- 620 IJ 11. IUnknown (Alkyt- Hydrocarbon) P82.91 I "2L J-JB- 12. IUnknown (sat'd Hydrocarbon) I 30.55 I410 1 3 13. IUnknown (sat'd Hydrocarbon) I 32.61 I400 1 . 114. Iunknown I 33.75 4201. I 15.III 116. __ _ _ _ _ _ _ _ _ _.._ _ _ _1_ _ _ _1_ _ I 17.L__ _ _ _ _ _ _ _ _ _I_ _ _ _I_ _ _ _I_ _ _ 118. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 19._ _ _ _ _ _ __ _ 1_ _ _ _1 _ _ _ _ _ 120.1__ _ _ _ _ _ _ _ _ _ __ _ _ _I_ _ _ _ I__ _ I I21. _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ 1 _ _ _ _ 1 _ _ _ _ _1_ _ _ 122. _ _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ _ _ _ _I_ _ _ 123. _ _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ _ _ _ _I_ _ _ 124. J_ _ _ _ _ _ _ _ _ _ _ _ _ _ _]_ _ _ _ _ _ 125. _ _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ _ _ _ _1_ _ _ 126. _ _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ _ _ _ _I_ _ _ 127.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ _1_ _ _ _ 1__ _ 128. _ _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ _ _ _ _1_ _ _ 129.1 __ _ _ _i_ _ _ _ __ _ 130. i_ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ _ _ _ _ _ _I_ _ _ Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the samp~te. B-Analyte was found in the reagent blank as well as the sample. J3 - Indicates an estimated value. NO - Not detected. A -Aldol condensation product. D - secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D- 22
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 1 AnaLIS ID: 901206-020 Customer Sample ID: N-102 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSMER/R. SHUCK File ID: 07598 Samle Matrix: SOIL instrument ID: 597012 Re~iisition Nmbe~r: Authorized By: 0. C. Canada Date Sample Received: 5-OEC-1990 VOA - Volatile, Organic Compounds (TCL) Date Extracted/Prepared: Date Analyzed: 10-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Number: VGA (CLP) MOP Percent Moisture: 8 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: SL STAFFORD Associated Blank: 901210-025 GA Fite Number: MA U:Result has been Corrected for Spike CAS ug/Kq CAS ug/Kg ......................... .......... ........... .............................. .......... 74-87-3 ChLoromethane 1IU 79-00-5 1,1.2-Trichtoroethane 5U 74-113-9 Bromomethane 11U 71-43-2 Benzene 5u 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1.3-Dichloropropene 5U 75-00-3 Chtoroethane 111U 75-25-2 Bromoform 5U 75-09-2 Methytene Chloride 5 -Q--ft LA 108-10-1 4-Methyt-2-pentenone llu 67-64-1 Acetone 30-1. Ik 591-78-6 2-Nexanone 11U 75-15-0 Carbon DisuLfide 5U 127-18-4 Tetrachloroethene 5U 75-35-4 1.1-Dichloroethene 5U 79-34-5 1.1.,2-TetrachLoroethane 5U 75-34-3 1*1-Dichtoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-DichLoroethene (total) 5U 108-90-7 Chlorobenzene su 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichloroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1lelelTrichioroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichtoromethane 5U 78-87-5 1,2-Dichtoropropane 5U 10061-01-5 cis-1,3-Dichloropropene 5UA 79-01-6 Trichloroethene 5U 1 /43, 124-48-1 Dibromochtoroinethane 5U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. 8B Analyte was founad In the reagent blank as well as the sample. J1 - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D- 23
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