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WHC-SD-EN-TI-136, Rev, 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS 10: 901206-020 Customer Sample 10: N-102 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSUER/R. SHUCK File 10: 10647 .Sample Matrix: SOIL Instrument 10: 597003 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BRA - Base/NeutraL/Acid Compounds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Numb~er: Analysis Procedure Number: BNA (CLP) HOP Percent Moisture: 7.7 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 aA Fite Number: UA [U : Result has been Corrected f or Spike CAS ug/Kg CAS ug/Kg ...... ..................... .......... ........... .............................. .......... 108-95-2 Phenol 99OU 106-47-8 4-Chtoroanitine 990U 111-44-4 bis(2-ChLoroethyl)ether 990U 87-68-3 HexachLorobuitadiene 990u 95-57-8 2-ChlorophenoL 99OU 59-50-7 4-ChLoro-3-methyiphenot 990u 541-73-1 1,3-DichLorobenzene 99OU 91-57-6 2-MethylnaphthaLene 990u 106-46-7 1,4-Dichiorobenzene 99OU 77-47-4 HexachLorocyclopentadiene 990U 100-51-6 *enzyl Alcohol 990U 88-06-2 2,4,6-TrichLorophenoL 990U 95-SO-1 1,2-OlchLorobenzene 99OU 95-95-4 2,S,-Trichlarophenot 4800u 95-48-7 2-Methyiphenot 99OU 91-58-7 2-Chtoronaplithatene 990u 108-60-1 bis(2-ChLoroisopropyt)ether 990U 88-74-4 2-IditroaniLine 480OU 106-44-5 4-Nethytphenot 990U 131-11-3 DimethyLpinhatate 990u 621-64-7 N-Nitroso-di-n-propylamine 990U 208-96-8 Acenaplithylene 990U 67-72-1 Hexachtoroethane 990U 99-09-2 3-NitroaniLine 480OU 98-95-3 Nitrobenzene 9901U 83-32-9 Acenaphthene 990U 78-59-1 Isophorone 990U 51-28-S 2,4-Dinitrophenot 480OU 88-75-S 2-Nitrophenot 990U 100-02-7 4-Witrophenol. 480OU 105-67-9 2,4-DimethyLphenol 99OU 132-64-9 Dibenzofuran 990U 65-85-0 *enzoic Acid 11'Q 489-do-. LA 121-1U-2 2,4-Dinitrotoluene 990U 111-91-1 bisC2-Chloroethoxy)methane 990U 606-20-2 2, 6 -Oinitrototuene 990U 120-83-2 2,4-Dichlorophenol 990U 84-66-2 Diethylphthalate 9)90 2~0-. 6 A 120-82-1 1,2,4-Trichtorobenzene 990U 7005-72-3 4 -Chtorophenyt-phenyLether 990U 91-20-3 Naphthalene 99OU 86-73-7 I'Luorene 990U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number Is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D- 20
WIIC-S-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaL!! ID: 901206-020 Customer Samle ID: N-102 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSWER/R. SHUCK Fite ID: 1064.7 Sample Matrix: SOIL Instrument ID: 5970#3 Requisition Number: Authorized By: D. C. Canada Date Samuple Received: 6-DEC-1990 DNA -*ase/Neut ratl/Acid copounads (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Number: Analysis Procedure Number: BNA (CLP) MOP Percent Moisture: 7.7 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C 1MEEMAN Associated Blank: 901213-028 QA File Number: NA [I : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ...... .................. .......... ........... .............................. .......... 100-01-6 4-Nitroaniline 4800Uj 53-70-3 Dibenz(a~h)anthracene 990U 534.-52-1 4,6-Dinitro-2-methylphenol 4800U 191-24-2 Uenzo(g,h,i)perylene 990U 86-30-6 N-Nltrosodiphenylamine 99OU 101-55-3 4-Uromopheny-phenylether 990Ui 118-74-1 HexachLorobenzene 990U 87-86-5 PentachLorophenol 4800ui 85-01-8 Phenanthrene 990Ui 120-12-7 Anthracene 990Ui 84-74-2 Di-n-butylpdhthaLat* 32001k, Lk. 206-44-0 Fluoranthene 990U 129-00-0 Pyrene 9901J 85-68-7 Dutytbenzylphthatate 990U 91-94-1 3,3'-Olchlorobenzidine 2000Ui 56-55-3 Bonzo~a)anthracene 990U 117-81-7 bis(2-Ethythexyl)phthaLate 420 jo- 990 ) 218-01 -9 Chrysene 990U 117-84-0 Di-n-octylphthalate 990U 205-99-2 Uenzo(b)f luorantherve 990U 207-08-9 Benzo(k)fluoranthene 990U 50-32-8 Senzo(a)pyrene 990U 193-39-5 indeno(l,2,3-cd)pyrene 990U Data Reporting Qualifiers: U - Compounid was analyzed for but not detected. The number is the attainable detection Limit for the samrple. 6 - Analyte was foun~d In the reagent blank as well as the samrple. J - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. o - Secondary dilution. E - Exceeds initial calibration range. D-21
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