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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-038 Customer Sample ID: N-118 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SNUCK Sample Matrix: SOIL File ID: ),14467 Level: (low/mad): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. 7.1 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxM PH: ____ GPC Cleanup: (YIN) N Concentration Units Number TICs found: 17 CugIL or ug/Kg): uVK2 ICAS NUMBER j COMPOUND NAME RT IEST. CONC. a I ===i= ........... Z .. =-= ... l ....... ....- I . I... 1. 123-42-21 2-Pentanone._4-hydroxv-4-methy 3 .0v i 1T00I JA 12. 1 UNKNOWN 6.051 500 1 I3. 1 UNKNOWN ALCOHOL 4--.-Z.j.Ja. A ; I4. IUNKNOWN ALCOHOL I 13.88 3000jJ I5. 6. 7. IUNKNOWN IUNKNOWN IUNKNOWN HYDROCARBON I;.2 I 4?6f-.---4ej89______ ___ _____________ 2I F ______ ____ 19. 10. I11. 12. 8. IUNKNOWN HYDROCARBON IUNKNOWN jUNKNOWN HYDROCARBON UNKNOWN HYDROCARBON [UNKNOWN HYDROCARBON ~I7 I 24.841 26.7.I~ 27 I 49 ____ ps-____ 460j. 1 i ~ 'I' j I 13. [UNKNOWN HYDROCARBON 2~7 & r74- I 9 I- 14"._____ UNKNOWN HYDROCARBON 298 -4004-411. 15. I16. UNKNOWN HYDROCARBON UNKNOWN ALKOXY COMPOUND 1 j 30700 3i.09 99 i do 2089 d. 17. 118. 119. 120. 121. IUNKNOWN PHTHALATE ESTER I.._ .I_ j 32.37 _ _ _ _1_ 1__ _ _ _ __ _ _ _1_ _ _ _ _1_ 1100 I 1 _ _ _ _ _ _ _ _ _ 1__ _ _ _ _1_ _ _ I _ _ I 122.1__ _ _ _1_ _ _ _ 1__ _ 123. I_____I____ __ _ 124.II__ _ _ _I_ _ _ _ I__ _ I 125. I __ _ _ _I_ _ _ _ I__ _ I 126. I__ _ _ _I_ _ _ _ I__ _ I 127. I. _ _ _ _1_ _ _ _ _ _ 128.II__ _ _ _1_ _ _ _ 1__ _ I 129. ____ I___I 130. j____ I Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sampte. 6-Analyte was found in the reagent blank as well as the sample. J Indicates an estimated value. ND Not detected. A - AldoL condensation product. D - Secondary dilution. E -Exceeds initial calibration range. P - Probable Identification. D-86
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of I AnaLIS ID: 901206-038 Customuer Sampte ID: N-118 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07588 Semple Matrix: SOIL Instrument ID: 597002 Requjisition Numb~er: Authorized By: 0. C. Canada Date Sape Received: 5-DEC-1990 VDA - Volatile Organic Compounds CTCL) Date Extracted/Prepared: Date Analyzed: 10-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Nuumber: VOA (CLP) NOP Percent Moisture: 7 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: SL STAFFORD Associated Blank: 901210-025 CA Fite Numiber: NA El : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 74-87-3 Chloromethane 11U 79-00-S 1,1,2-Trichloroethane SU 74-83-9 Bromomethane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichloropropene 5U 75-00-3 Chtoroethane 11U 75-25-2 Bromoform 5U 75-09-2 Methylene Chloride 5- 9- (A 108-10-1 4-Methyt-2-pentanone 1lU 67-64-1 Acetone 11U 591-78-6 2-Nexanone 11U 75-15-0 Carbon Disulfide 5U 127-18-4 TetrachLoroethene 5U 75-35-4 1,1-oichtoroethene SU 79-34-5 1,1.2,2-TetrachLoroethane 5U 75-34-3 1,1-Dichioroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichloroethene (total) 5U 108-90-7 Chlorobenzene SU 67-66-3 Chloroform 5U 100-41-4 EthyLbenzene 51) 107-06-2 1,2-Dichtoroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-Trichtoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichtoromethane 5U 78-87-5 1,2-Dichloropropane 5U 10061-01-5 cis-1,3-Dichtoropropene 5U 79-01-6 Trichloroethene 5U / 124-48-1 Dibromochtoromethane 5U Data Reporting Qualifiers: U - Compoun~d was analyzed for but not detected. The nu~mber is the attainable detection limit for the salmpte. 8 - Analyte was found in the reagent blank as well as the sampte. J - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-87
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