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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLiS ID: 901206-030 Customer Sample ID: N-110 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNERIR. SHUCK Fite 1D: 10659 Sample Matrix: SOIL Instrumnent ID: 597093 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BNA -Base/Neutral/Acid Compounzds CTCL) Date Extracted/Prepared: IZ-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Nuber: Analysis Procedure Number: UNA CCLP) MOP Percent Moisture: 7.4 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 GA File Number: NA U:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ............................ .......... ........... .............................. .......... 100-01-6 4-Nitroanitine 4800U 53-70-3 Dibenz~a,h)anthracene 991. 534-52-1 4.6-Dinitro-2-methylphenol 4800U 191-24-2 Benzo(g~hJi)perylene 991. 56-30-6 N-Nitrosodiplienylamine 990U 101-55-3 4-Bromopheyl-phenylether 990U. 118-74-1 Hexachlorobenzene 990U 87-86-5 Pentachtorophenol 480OU 85-01-8 Phenantht-ene 990U 120-12-7 Anthracene 991. 84-74-2 Di-n-butylphthaLate 1800'S.. Li. 206-44-0 Fluoranthene 991. 129-00-0 Pyrene 99OU 85-68-7 Butylbenzylphthalate 990U 91-94-1 3,3'-Dichiorobenzidine 2000U 56-55-3 Benzo~aenthracene 990u 117-81-7 bisC2-Ethythexyl)phthaLate 389-" -IC 09 LA, 218-01-9 Chrysene 990k) 117-84-0 Oi-n-octylphthelate 990U 205-99-2 Benzo(b)ftuoranthene 990U 207-08-9 Benzo(k)fluoranthene 990U 50-32-8 Benzo(a)pyrene 990U 193-39-5 Indeno(1,2,3-cd)pyrene 990U Data Reporting Qualifiers: U Comipounid was analyzed for but not detected. The number is the attainable detection limit for the sample. B -Analyte was foun~d in the reagent blank as well as the sample. J -Indicates an estimated value. NO -Not detected. A -Aldol condensation product. D Secondary dilution. E -Exceeds initial calibration range. D- 50
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BRA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPUNDS AnaLIS ID: 901206-030 Customer Sample ID: N-110 Laboratory: Organic Mass Spectroscopy Laborotor Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File IDN 10659 Level: Clow/med): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. 7.4 dec. _____Date Extracted: 12-DEC-1990 Extraction: (SepFICont/Sonc) SoxH PH: - GPC Cleanup: (Y/N) N Concentration Units Number TIC& found: 12 CugIL or uglKg): gxLK CAS NUMBER COMPOUND NAME RT IEST. CONC. I 0 I1. I2. 141-79-71 3-Penten-2-one, 4-methyl- 123-42-21 2-Pentanone. 4-hydroxy-4-methy 4.92 I49" -b..O " 1 JIA I3. 872-50-41 2-Pyrrolidinone. 1-methyt- I4. IUnknown (sat'd Hydrocarbon) I5. IUnknown (sat'd Hydrocarbon) I6. IUnknown (Hydrocarbon) I7. IUnknown (sat'd Hydrocarbon)j I8. IUnknown 1 I9. jUnknown (Hydrocarbon) 110. jUnknown (Hydrocarbon) 1 I 1.jUnknown (Hydrocarbon) I 9 .E:I'6 2 19.43 I660 J 256 86 j0- 25.89 I850 IJ u.I 27.671 1500 1 pe.i[ I .490-+. .n 30.531 410j 1 32.60 1420 J . / 6 12. JUnknown (Hydrocarbon) I 33.45 I 1300I I 113. _ __ _1III I14.__ _ _ _ j II I15.__ _ _ _ j II 116. ____ 117. 1___ 118. ____ 119. ____ 120.j II 121.11____1 122. 11____1____1___ 123.1____1____1 I 24. 1____1____1___ 125. I1____1____I___ 126. 1_ _ _ _. _ _ _ 1__ _ I 127. II____I____I___ 128. - I____ ____I___ 129. _____I____i___I 130. I Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The nu~mber Is the attainable detection limit for the samp~le. 8 - Anolyte was found in the reagent blank as well as the sample. j - Indicates an estimated value. RD - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds Initial calibration range. P - Probable Identification. D-51
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P.O. Box 1970 Rfichland. WA 99352 W
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