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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 2 AnaLIS ID: 901206-034. Customer Snmple ID: N-114 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite 10: 10663 Samp~le Matrix: SOIL instrument 10: 5970#3 Requisition N~.uber: Authorized By: 0. C. Canada Date Sample Received: 6-DEC-1990 DNA - Dase/Neutral/Acid Compounds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14.-DEC- 1990 Preparation Procedure Numiber: Analysis Procedure Numb~er: ORA (CLP) MOP Percent Moisture: 3.3 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 CA File Number: NA D : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .................................. .......... ........... ............................... .......... 108-95-2 Phenol 8801. 106-4.7-8 4-Chioroanitine 881. 111-4.4-4. bis(2-Chloroethyl)ether 880U 87-68-3 Hexachtorobutadiene 880U 95-57-8 2-Chlorophenot soot) 59-50-7 4-Chloro-3-methylphenot 881. 54-73-1 1,3-Oichlorobenzene 880U 91-57-6 2-Methyinaphthatenve 880U 106-46-7 1,4-Dichiorobenzene SB0U 77-47-4 Nexachlorocyclopentadiene 880U 100-51-6 Benzyt Alcohol 880U 88-06-2 2,4,6-Trichlorophenot 880U 95-50-1 1,Z-Dichlorobenzene 881. 95-95-4 2.4,5-TrichLorophenot 4201. 95-48-7 2-Methylpienol 880U 91-58-7 2-Chloronsphthalene 880U 108-60-1 bisC2-Chloroisopropyt)ether Book) 88-74-4 2-Nitroaniline 420OU 106-44-5 4-Methylphenol 8801. 131-11-3 Dimethylphthalate 881. 621-64-7 N-Nitroso-di-n-propylemine 880U 208-96-8 Acenaphthylene 880U 67-72-1 Nexachloroethane 880U 99-09-2 3-Nitroaniline 4201. 98-95-3 Nitrobenzene 880U 83-32-9 Acenaphthene 880U 78-59-1 isophorone 8801. 51-28-5 2,4-Dinitrophenol 42001U 58-75-5 2-Nitrophenol 880U 100-02-7 4-Nitrophenol 4201U 105-67-9 2,4-ODimethytpIhenot 880U 132-64-9 Dibenzofuran 880U 65-85-0 Benzoic Acid 6W0 "e-19 LA 121-14-2 2,4-Dinitrotoluene 88OU 111-91-1 bisC2-Chloroethoxy)methane 8U 606-20-2 2.6-Dinitrototuone 88OU 120-83-2 2.4-Dichlorophenot 880U 84-66-2 iethylphthelate Sao-aqe-W~ L4A 120-82-1 1,2,4-Trichiorobenzene 880U 7005-72-3 4-Chlorophenyt-phenylether 881. 91-20-3 Naphthalene 881. 86-73-7 Fluorene 880U. Data Reporting Oualiffiers: U -Compound waas analyzed for but not detected. The numb~er is the attainable detection limit for the sample. B -Analyte was found in the reagent blank as waelt as the sample. J -Indicates an estimated value. ND -Not detected. A -Aldol condensation product. D -Secondary dilution. E -Exceeds initial calibration range. D -66
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLiS ID: 901206-034 Customer Sample ID: N-114 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 10663 Sample Matrix: SOIL Instrument ID: 597083 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BRA - Base/Neutral/Acid Compounds (TEL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-IM9 Preparation Procedure Numbr: Analysis Procedure Number: DNA (CLP) NOP Percent Moisture: 3.3 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEENAN Associated Blank: 901213-028 QA File Number: NA [] : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 100-01-6 I-NitroaniLine 4200U 53-70-3 .Dibenz(a~h)anthracene 88OU 534-52-1 4,6-Dinitro-2-methylphenot 420OU 191-24-2 Denzo~g,h.i)perylene 88OU 86-30-6 N-Nitrosodiphenylamine 880U 101-55-3 4-oramopiheny-phenytether 881. 118-74-1 Nexachlorobenzene 881. 87-86-5 Pentachlorophenol 4200U 85-01-8 Phenanthrene 881. 120-12-7 Anthracene BBOU 84-74-2 0i-n-buitylphthalate 2900-5, l.A 206-44.-0 Fluoranthene 880U 129-00-0 Pyrene 881. 85-68-7 Dutyibenzylphthalate 88OU 91-94-1 3,3'-Dichlorobenzidine 1800U 56-55-3 Benzo(a)anthracene 881. 117-81-7 bis(2-Ethylhexyt)plithalate -250il% 880 LA, 218-01-9 Chrysene 880U 117-84-0 Di-n-octylphthalate 88OU 205-99-2 genzo(b)fluorenthene 880U 207-08-9 Denzo(k)fluoranthene 881. 50-32-8 Renzo(a)pyrene 881. 193-39-5 Indeno(1,2,3-cd)pyrene S80U Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The number Is the attainable detection limit for the sampLe. * Analyte was found in the reagent blank as well as the sample. J1 Indicates an estimated value. NDO Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D -67
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