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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of I AnaLiS ID: 901206-049 Customer Sample ID: N-126 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07637 Sample Matrix: SOIL Instrument ID: 597002 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VOA -Volatile Organic Compounds CTCL) Date Extracted/Prepared: Date Analyzed: 12-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Numb~er: VOA CCLP) NOP Percent Moisture: 8 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL HUDDLESTON Associated Blank: 901212-004 QA File Niuber: NA C] : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ...... ........................... .......... ........... .............................. .......... 74-87-3 Chtoromethane 11U 79-00-5 1,1,Z-Trichioroethane SU 74-83-9 Uronmmthane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichtoropropene SU 75-00-3 Chloroethane 11U 75-25-2 Bromnoform 5U 75-09-2 Methylene Chloride 109.3. LAk 108-10-1 4-Methyt-2-pentanone 11U 67-64-1 Acetone 54'S. LA 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachtoroethene 5U 75-35-4 1,1-Dichloroethene 5U 79-34-5 1,1.2,2-Tetrachtoroethane 5U 75-34-3 1,1-Dichloroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichloroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-DichLoroethane SU 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) SU 71-55-6 1,1,1-Trichtoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichtoromethane SU 1006-01-5 c1,3-Dichorropone 5U 7806-87-S 79-01-6 124-48-1 c1-Dichloroprne Trichloroethene Dibromochioromethane 5U 5U 5U 6 7 q Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. * - Analyte was found in the reagent blank as well as the sample. J- Indicates an estimated value. RD - Not detected. A - Aldol condensation product. 0 - Secondary dilution. E - Exceeds initial calibration range. D-120
WHC-S-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS ID: 901206-050 Customer Sample ID: N-127 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fit. ID: r14481 Sample Matrix: SOIL Instrument 1D: HP-5985 Requisition Numiber: -Authorized By: 0. C. Canada Date Samp~le Received: 5-DEC-1990 BRA - Base/Neutral/Acid Comp~ounds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 3-JAN-1991 Preparation Procedure Number: Analysis Procedure Number: BHA (CLP) MOP Percent Moisture: .1 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Slank: 901214-083 QA File Number: NA H : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ............................... .......... ........... .............................. .......... 108-95-2 Phenol 960UJ 106-47-8 4-ChLoroanilne 960U5 111-44-4 bis(2-ChtoroethyL)ether 960U _ 87-68-3 Hexachlorobuztediene 960U 3 95-57-8 2-ChLorophenol 960U .7 59-50-7 4-Chloro-3-methylphenol 960U-1 541-73-1 1,3-Dichlorobenzene 960) 91-57-6 2-Methytnephthalenve 96OU 7 106-46-7 1,4-Dichlorobenzene 960U Y 77-47-4 Hexachlorocyctopentadiene 960UJ' 100-51-6 Benzyl Alcohol 960U 7 88-06-2 2,4,6-TrichLorophenot 960U 7 95-50-1 1,2-Dichlorobenzene 960U j 95-95-4 2,4.5-Trichlorophenol 480DU J 95-48-7 2-Methyiphenoi 960U7j 91-58-7 2-Chtoronaphthalene 960U 7 108-60-1 bisC2-Chloroisopropyt)ether 960U 7 88-74-4 2-Nitroaniline 4800 11 106-44-5 4-Methytphenot 960U 7 131-11-3 Dimethytplithatate 96DU Jr 621-64-7 N-Nitroso-di-n-propylamine 960U T 208-96-8 Acenaphthylene 960U X 67-72-1 Hexachloroethane 960U3- 99-09-2 3-Nitroaniline 4800U j 98-95-3 Nitrobenzene 960U-Y 83-32-9 Acenaphthene 960UT 78-59-1 Isophorone 960U X 51-28-5 2,4-Dinitrophenol 4800U,7 88-75-5 2-Nitrophenol 960U 3 100-02-7 4-Nitrophenol 4800U 7 105-67-9 2,4-Dimethylphenol 960U T 132-64-9 Dibenzofuran 960U Z 65-85-0 Benzoic Acid 4800U T 121-14-2 2,4-Dinitrototuene 960U 7 111-91-1 bis(2-Chloroethoxy)methane 960U 7 606-20-2 2,6-Dinitrotoluene 960U3r 120-83-2 2,4-Dichlorophenol 960UT 84-66-2 Diethytphthatate 960U.17 120-82-1 1,2,4-Trichlorobenzene 960U 7 7005-72-3 4-Chtorophenyl-phenylether 960U 7 91-20-3 Naphthalene 960U J 86-73-7 Fluorene 960U 3 Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the samrple. B - Analyte was found in the reagent blank as well as the sanipte. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-121
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P.O. Box 1970 Rfichland. WA 99352 W
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