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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 1 AnaLlS ID: 901206-04.4 Customer Sample ID: N-122 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 07605 Sample Matrix: SOIL instrument ID: 597002 Requisition Numb~er: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VOA - Volatile Organic Compounds (TCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Number: PURGE 9 TRAP Analysis Procedure Numb~er: VGA (CLP) NOP Percent Moisture: 6 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL HUDDLESTON Associated Slank: 901211-004 OA File Number: NA (I:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ................... .............................. .......... ...........----------------.......... 74-87-3 Chtoromethane 11U 79-00-5 1,1,2-Trichtoroethane 5U 74-83-9 Bromomethane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Oichtoropropene 5U 75-00-3 Chtoroethane 11U 75-25-2 Bromoform 5U 75-09-2 Methylene Chloride 5U 108-10-1 1-Methyl-2-pentanone llU 67-64-1 Acetone 11U 591-78-6 2-Hexanone 11U 75-15-0 Carbon DisuLfIde 5U 127-18-4 TetrachLoroethene 5U 75-35-4. 1,1-Dichtoroethene 5U 79-34-5 1.1,2,Z-Tetrachloroethane 5U 75-34-3 1,1-Dichtoroethane SU 108-88-3 Toluene 5U 540-59-0 1,2-Dichtoroethene (total) 5U 108-90-7 ChLorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 EthyLbenzene 5U 107-06-2 1,2-Dichtoroethane SU 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-Trichloroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-1. Vinyl Acetate 11U 75-27-4 Bromodichtoromethane 5U 78-87-5 1,2-Dichloropropane SU 10061-01-5 cis-1,3-Dichloropropene SU 79-01 -6 Trichloroethene 5U 124-48-1 Dibromochloromethane 5U Data Reporting Cualifiers: U - Comrpound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J2 - Indicates an estimated value. No - not detected. A - Aldol condensation product. O - Secondary dilution. E - Exceeds initial calibration range. D-104
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS 10: 901206-045 Customer Sample ID: N-123 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 3141.74 Sample Matrix: SOIL Instrument ID: HP5985 Requisition Number: Authorized By: 0. C. Canada Date Sample Received: 5-DEC-1990 BNA - Base/Neutral/Acld Compoun~ds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Nuber: Analysis Procedure Number: SNA (CLP) HOP Percent Moisture: 8.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 OA File Nu~mber: NA 0] : Result has been Corrected for Spike CAS uglKg CAS ug/Kg ............................... .......... ........... .............................. .......... 108-95-2 Phenol ft IOOOU 106-47-8 4-ChloroaniLine R IOU 111-44-4 bis(2-ChLoroethyt)ether R 1000U 87-68-3 MexachLarobutadiene ft 1 000tU 95-57-8 2-ChlorophenoL R 1000U 59-50-7 4-Chloro-3-methylphenoL ft 1000U 541-73-1 1,3-Dichlorobenzene ft 1 000U 91-57-6 2-MothytnaphthaLene ft 1000U 106-46-7 1.4-Dichtorobenzene ft 000t; 77-47-4 Hexachlorocyclopentadiene Rt 100OU 100-51-6 Benzyt Alcohol ft 100OU 88-06-2 2,4,6-Trichlorophenot ft 100OU 95-50-1 1,2-Dichlorobenzene ft 1 000tU 95-95-4 2,4,5-Trichlorophenol ft 5200t) 95-48-7 2-Methytphenol ft 100OU 91-58-7 2-ChLoronaphthatene ft 1000U 108-60-1 bls(2-Chlorolsopropyl)ether ft 1 000tU 88-74-4 2-Nitroaniline Rt 520OU 106-44-5 4-MethytphenoL ft 1000U 131-11-3 Dimethylphthalate ft 100OU 621-64-7 N-Witroso-di-n-propylamine Rt I000U 208-96-8 Acenaphthylene ft 1000U 67-72-1 Hexachtoroethane ft 1000U 99-09-2 3-Nitroanitine ft 520OU 98-95-3 Nitrobenzene ft 1000U 83-32-9 Acenaphthene ft 1000U 78-59-1 Isophorone ft I000tU 51-28-5 2,4-Dinitrophenol ft 5200U 88-75-5 2-NitrophenoL ft 1000U 100-02-7 4-Nitrophenol ft 5200u 105-67-9 2,4-DimethytphenoL ft IOOOU 132-64-9 Dibenzofuran R I000U 65-85-0 Benzoic Acid ft 5200U 121-14-2 2,4-Dinitrotoluene ft 1000U 111-91-1 bis(2-Chloroethoxy)methane ft 1000U 606-20-2 2,6-Dinitrotoluene Rt 1000U 120-83-2 2,4-Dichlorophenol ft 1000U 84-66-2 Diethylphthalate Rt 1000U 120-82-1 1,2,4-Trichlorobenzene ft 1000U 7005-72-3 4-Chtorophenyt-phenyLether ft 1 000U 91-20-3 Naphthalene ft 1000U 86-73-7 FLuorene Rt IOOOU Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the samrple. B - Analyte was found in the reagent blank as well as the sample. J1 - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds Initial calibration range. D-105
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