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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-050 Customer Sample ID: N-127 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File IN: 314481 Samwple Matrix: SOIL Instrumient ID: NP-5985 Requisition Number: Authorized By: 0. C. Canada Date Sample Received: 5-DEC-1990 BRA - Base/Neutral/Acid Compounmds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 3-JAN-1991 Preparation Procedure Numb~er: Analysis Procedure Number: BNA (CLP) HOP Percent Moisture: .1 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK NEADRICK Associated Blank: 901214-083 OA File Numb~er: NA II:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ..................---------------- .......... ........... .............................. .......... 100-01-6 4-Nitroaniline 480OUZY 53-70-3 Dibenz(a~h)anthracene 960U7 534-52-1 4,6-Dinitro-2-methylpienot 4800U 7 191-24-2 Benzo(g~h,l)perylene 960U j 86-30-6 N-Nitrosodiphenylamine 960U 3 101-55-3 4-Bromophenyt-pIhenytether 960Uj 118-74-1 Nexachlorobenzene 960U:T 87-86-5 Pentachlorophenol 4800U 1 85-01-8 Phenanthrene 960Uj 120-12-7 Anthracene 960U 7 84-74-2 Di-n-butylphthalate 25001L Lk-y 206-44-0 Fluoranthene 96OU J- 129-00-0 Pyrene 960U 7 85-68-7 Butylbenzylphthalate 960U 7 91-94-1 3,3'-Dichlorobenzidine 2000U IT 56-55-3 Benzo(a)anthracene 960U.T 117-81-7 bis(2-Ethythexyl)phthalate 960U 3 218-01-9 Chrysene 960U 7 117-84-0 Di-n-.octylplithalate 960U T 205-99-2 Benzo(b)ftuoranthene 960U 3 207-08-9 Benzo(k)fluoranthene 960UT 50-32-8 Benzo~a)pyrene 960U,17 193-39-5 Indeno(1.2,3-cd)pyrene 960UJ ' Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numiber is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - indicates an estimated value. RD - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-122
WHC-S-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department SNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-050 Customer Sample ID: 11-127 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL Fite ID: >144.81 Level: (Low/med): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 3-JAN-1991 % Moisture: not dec. .1 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxH PH: ____ GPC Cleanup: (YIN) N Concentration Units Number TICs found: 20 Cug/L or ug/Kg): _uL~ I CAS NUMBER I COMPOUND NAME RT IEST. CONC. j~zXX 1 = ==~z* ZZS23232.2..Zzu : =: I I..z 12C33221 ==z~ 1. I2. I3. I4. I5. 6. I7. I8. I9. 123-42-21 2-Pentanone. 4-hydroxy-4-methy 1 UNKNOWN ALCOHOL 1 UNKNOWN 1 UNKNOWN IUNKNOWN IUNKNOWN IUNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN PHTHALATE ESTER j L j j I23.88 U=4-44&.-. IO 16.9O------0O-... ~ 19I.S. i8 j~ 20c.88j -48064-n- 2I? 64 1390 J mte I (10. I11. jUNKNOWN jUNKNOWN HYDROCARBON I 24.86! 23.00 1 5501 66e 12. jUNKNOWN AROMATIC KETONE 26.9i 70 3 13. jUNKNOWN HYDROCARBON Z6.34 14. 15. 116. jUNKNOWN HYDROCARBON jUNKNOWN HYDROCARBON [UNKNOWN j j PA o.lu 29.701 4.5 500-1 .. o )0IJ 8801 I 17. IUNKNOWN HYDROCARBON j 2.?9 liI . de- 18. 19. I20. (21.1 IUNKNOWN HYDROCARBON IUNKNOWN ALKOXY COMPOUND IUNKNOWN PHTHALATE ESTER I j 308 I ).&0 32.36 I1400 1 I 44GOI IJ I (22. ___________________ (23. (24. 125.1III 1_ J _ _ _ _ _ _ _ _ _ _ (26. (27. III I I (28.1 I 29.__ _ _ II 130. I Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection Limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J- Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D-123
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