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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department SNA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPUNDS AnaLIS ID: 901206-034 Customer Smple I0: N-114 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sape Matrix: SOIL File I0: 10663 Level: (low/med): LO Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. 3.3 dec. _____Date Extracted: 12wDECw1990 Extraction: CSepFIContISonc) SoxH PH: ____ PC Cleanup: (YIN) N Concentration Units Number TICs foun~d: 14. CugIL or uglKg): _ug/~ ICAS NUMBER ICOMPOUND NAME R T EST. CONC. 0 I1. 123-4.2-21 2-Pentanone, 4-hydroxy-4-methy I2. 872-50-41 2-Pyrrotidinone, 1-methyt- I3. 25013-16-51_Phenol.(l.1-dimethylethyt)-4-m I4. 17851-53-51 1.2-genzenedicarboxylic acid.b I I 5 .9i 9.&1- 46r el.29 AW0 0 09 -O 4" §, "0. is~Qj 52 0% . I5. I6. IUnknown (sat'd Hydrocarbon) Lunknown 1 -2-6 I7dOj~ 21.931 39 3701 /7 a . jUnknown (Alkyl Hydrocarbon) 1r [3.7 )IJ1 I9. Unknown (sat'd Hydrocarbon) 29.9970I 10. junknown 1 25.96 I620 1 J I11. 12z. 13. jUnknown (sat'd Hydrocarbon) lUnknown IUnknown (Atkyl Hydrocarbon) .1 I 3.efI3- 27.68j . ;; - IJO& 2800 j 400 j-d 114. Iunknown I 33.741 6101 J 116. II 119. III 120. I_ _ _ _ _ _ _ _ _ _ _ 121. I_ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ _ _ 122. __ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ 1 _ _ 123. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ 124. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ 125.1__ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _1_ _ _ _ _1_ _ _ I 126.1__ _ _ _ _ _ _ _ _ _ _ 1 _ _ _ _1_ _ _ _ 1 _ _ I 127. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ 128. 1- ____I____ __ 129. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ _ _ 130.j I I Data Reporting Qualifiers: U Compound waas analyzed for but not detected. The number is the attainable detection limit for the sample. B -Analyte was founrd In the reagent blank as well as the sample. J -Indicates an estimated value. NO -Not detected. A Aldol condensation product. D -Secondary dilution. E Exceeds initial calibration range. P -Probable Identification. D-68
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 1 AnaLtS ID: 901206-034 Customer Sample ID: M-114. Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07618 Sample Matrix: SOIL Instrumnent ID: 597052 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VGA -Volatile Organic Compounds (TCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Numiber: PURGE & TRAP Analysis Procedure Number: VOA CCLP) NOP Percent Moisture: S Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL HUDDLESTON Associated Blank: 901211-004 QA File Number: NA El : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 74-87-3 Chloromethane 11U 79-00-S 1,1.Z-Trichtoroethane 5U 74-83-9 Bromomethane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1.3-Dichloropropene SU 75-00-3 Chloroethane 11U 75-25-2 Bromoform SU 75-09-2 Methylene Chloride 5U 108-10-1 4-Methyl-2-pentenone 11U 67-61 Acetone 12 L.A 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachtoroethene 5U 75-35-4 1,1-Dichloroethene 5U 79-34-5 1.1.2,2-Tetrachloroethane 5U 75-34-3 1*1-Dichtoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichloroethene (total) 5U 108-90-7 Chlorobenzene SU 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-DichLoroethane 5U 100-42-S Styrene 5U 78-93-3 2-Dutanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-Trlchloroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichtoromethane 5U 78-87-5 1,2-Dichioropropane SU 10061-01-5 cis-1,3-Dichloropropene 5U 79-01-6 Trichtoroethene 5U 124-48-1 Dibromochtoromethane 5U Data Reporting Qualifiers: 1 U -Compound was analyzed for but not detected. The number Is the attainable detection limit for the sample. * - Analyte was found in the reagent blank as well as the sample. J5 - Indicates an estimated value. NO - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D -69
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