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NASA Scientific and Technical Aerospace Reports

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27<br />

NONMETALLIC MATERIALS<br />

Includes physical, chemical, <strong>and</strong> mechanical properties of plastics, elastomers, lubricants, polymers, textiles, adhesives, <strong>and</strong> ceramic<br />

materials. For composite materials see 24 Composite Materials.<br />

20040111036 Musashi Inst. of Tech., Tokyo, Japan<br />

Measurement of Bulk Charge in Dielectric Materials Irradiated by Electron Beam in Vacuum Environment<br />

Osawa, N.; Takahashi, S.; Tanaka, Y.; Takada, T.; Watanabe, R.; Tomita, N.; Griseri, V.; Levy, L.; Laurent, C.; 8th Spacecraft<br />

Charging Technology Conference; March 2004; 7 pp.; In English; See also 20040111031; No Copyright; Avail: CASI; A02,<br />

Hardcopy<br />

Bulk charge accumulation in thin dielectric materials under electron beam irradiation in vacuum environment was<br />

observed using newly developed measurement system. Recently, some accidents in spacecraft due to the charging up of<br />

electric potential have been reported. Some of them are caused by surface discharge normally happens in plasma environment.<br />

Some others seem to be caused by discharge due to <strong>and</strong> an accumulation of charge in bulk of materials at relatively higher<br />

altitude environment. Surface charge is usually measured using surface potential meter. However, there had been no useful<br />

method to measure the bulk charge in the materials. Therefore, we have been developing the bulk charge measurement system.<br />

We have already succeeded in measuring the bulk charge distribution in thick sample under electron beam irradiation in air<br />

atmosphere. However, to simulate the actual spacecraft in condition of high altitude space environment, it is necessary to carry<br />

out the measurement for thin materials in vacuum environment. Therefore, we have developed an improved measurement<br />

system applicable to a thin sample in vacuum environment. Using the improved system, we carried out the measurement of<br />

bulk charge distributions in 180 <strong>and</strong> 50 m thick Kapton <strong>and</strong> PET film under electron beam irradiation in vacuum of ca 10-6<br />

Pa. In this report, some typical measurement results are introduced following the explanation of brief measurement principle.<br />

Author<br />

Charge Distribution; Dielectrics; Irradiation; Electron Beams; Vacuum<br />

20040111053 Musashi Univ., Tokyo, Japan<br />

Characteristic of Charge Accumulation in Glass Materials Under Electron Beam Irradiation<br />

Miyake, H.; Tanaka, Y.; Takada, T.; 8th Spacecraft Charging Technology Conference; March 2004; 9 pp.; In English; See also<br />

20040111031; No Copyright; Avail: CASI; A02, Hardcopy<br />

We observed space charge formation in various glass materials under electron beam irradiation. Spacecraft charging<br />

occurs in plasma <strong>and</strong> radiation environment. Especially we have focused on an accident caused by internal charging in glass<br />

material used cover of solar array panel. Therefore we have tried to measure the charge distribution in glass materials<br />

irradiated e-beam. The measurement is carried out using PEA (Pulsed Electro-Acoustic method) system. Two types of glass<br />

materials are used for samples. One is a quartz glass (pure SiO2), <strong>and</strong> another are glasses including impurities of oxide metal.<br />

In the case of quartz glass, charge accumulation was not observed neither during nor after electron beam irradiation. On the<br />

other h<strong>and</strong>, charge accumulation was observed in glass sample including metal-oxide impurities. We found the polarity of the<br />

observed charges in bulk depends on the content of impurities. To confirm the existence of which impurity dominates the<br />

polarity of the accumulated charge, we measured charge distribution in several glass materials including various metal-oxide<br />

impurities.<br />

Author<br />

Charge Distribution; Accumulations; Glass; Electron Beams; Irradiation; Silicon Dioxide<br />

20040111065 Applied Sciences, Inc., Cedarville, OH, USA<br />

Carbon Nanofiber-Filled Materials for Charge Dissipation<br />

Jacobsen, Ronald L.; Walters, Kent R.; Glasgow, D. Gerald; Wang, Chyi-Shan; 8th Spacecraft Charging Technology<br />

Conference; March 2004; 6 pp.; In English; See also 20040111031; No Copyright; Avail: CASI; A02, Hardcopy<br />

This work explores the possibility of using carbon nanofibers to create improved versions of antistatic <strong>and</strong> conductive<br />

polyimide (e.g. Kapton.) for use in satellite charge control <strong>and</strong> dissipation. Carbon nanofibers have superior properties making<br />

them a c<strong>and</strong>idate for this application, including very small diameter (to fit within a thin film), high aspect ratio (to form a<br />

network), moderate electrical conductivity, <strong>and</strong> excellent dimensional stability. Nanofibers in the diameter range from 60 - 200<br />

nm (as distinct from smaller nanotubes) are now available relatively cheaply <strong>and</strong> in quantity. The primary challenge in making<br />

polyimide films is achieving adequate dispersion of nanofibers. This is complicated both by the fact that the nanofibers are<br />

entangled as produced, <strong>and</strong> that they are not naturally well wet by the polymer, causing them to agglomerate during processing<br />

prior to polyimide film casting. This paper describes methods for surface modification of nanofibers, as well as size separation<br />

79

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