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KIRTLAND AIR FORCE BASE ALBUQUERQUE, NEW MEXICO ...

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APPENDIX C<br />

CONTENTS (Continued)<br />

Section<br />

Page<br />

5.1 Sampling Protocols .......................................................................................................... C-25<br />

5.2 Sample Volume, Holding Times, Containers, and Preservation ..................................... C-25<br />

6. SAMPLE CUSTODY AND RECORD-KEEPING ...................................................................... C-31<br />

6.1 Field Custody Procedures ................................................................................................ C-31<br />

6.1.1 Field Documentation ........................................................................................... C-31<br />

6.1.2 Transfer of Custody and Shipment ..................................................................... C-32<br />

6.2 Laboratory Custody Procedures ....................................................................................... C-33<br />

6.3 Record-keeping ................................................................................................................ C-34<br />

6.3.1 Field Records ...................................................................................................... C-34<br />

6.3.2 Laboratory Data Deliverables ............................................................................. C-34<br />

7. CALIBRATION PROCEDURES AND FREQUENCY .............................................................. C-37<br />

7.1 General ............................................................................................................................. C-37<br />

7.2 Responsibilities ................................................................................................................ C-37<br />

7.2.1 Analytical Laboratory Equipment and Instrumentation ..................................... C-37<br />

7.2.2 Field Equipment and Instrumentation ................................................................. C-37<br />

7.3 Out-of-Calibration Equipment ......................................................................................... C-38<br />

7.4 Calibration Procedures for Laboratory Equipment .......................................................... C-38<br />

7.5 Calibration Procedures for Field Equipment ................................................................... C-38<br />

8. ANALYTICAL PROCEDURES .................................................................................................. C-41<br />

8.1 Laboratory Analyses ........................................................................................................ C-41<br />

8.2 Field Analyses .................................................................................................................. C-42<br />

8.3 Method Detection, Quantitation, and Reporting Limits .................................................. C-42<br />

9. INTERNAL QUALITY CONTROL CHECKS ............................................................................ C-43<br />

9.1 Field Quality Control Checks .......................................................................................... C-43<br />

9.2 Laboratory Quality Control Checks ................................................................................. C-43<br />

10. DATA VALIDATION, REDUCTION, AND REPORTING ....................................................... C-47<br />

10.1 Data Validation ................................................................................................................ C-47<br />

10.1.1 Laboratory Data .................................................................................................. C-47<br />

10.1.2 10.1.2 Field Records ........................................................................................... C-48<br />

10.2 Data Reduction ................................................................................................................. C-49<br />

10.3 Reporting .......................................................................................................................... C-49<br />

11. PERFORMANCE AND SYSTEMS AUDITS ............................................................................. C-51<br />

11.1 General ............................................................................................................................. C-51<br />

11.1.1 Field System Audit ............................................................................................. C-51<br />

Kirtland AFB<br />

Quality Assurance Project Plan C-4 April 2004

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