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KIRTLAND AIR FORCE BASE ALBUQUERQUE, NEW MEXICO ...

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APPENDIX C<br />

procedures that may result in sample contamination. Trip blanks will be used to assess potential VOC<br />

contamination in water samples as a result of sample shipment and storage.<br />

Field QC samples will be collected as specified in the project-specific QAPP, and a minimum of five<br />

percent for field duplicates and equipment blanks. Trip blanks samples will accompany each cooler of<br />

water samples for VOC analysis. Ambient blanks for VOC analysis will be collected on a projectspecific<br />

basis.<br />

2.15 Laboratory Quality Assurance Program<br />

Laboratories performing work in support of Kirtland AFB will maintain current certification by USACE.<br />

AFCEE, or NELAP, as appropriate. In addition, the laboratories will maintain a current approved QAPP<br />

including standard operating procedures (SOPs) for the following:<br />

Sample receipt and logging<br />

Sample storage<br />

Preventing sample contamination<br />

Security for laboratory and samples<br />

Standards purity/preparation<br />

Maintaining instrument records and log books<br />

Sample analysis and data control systems<br />

Glassware cleaning<br />

Technical and managerial review of laboratory operation and data package preparation<br />

Internal review of QA and QC data<br />

Sample analysis, data handling, and reporting<br />

Chain-of-custody procedures and document control<br />

Laboratory data validation/laboratory self-inspection system<br />

Data management and handling<br />

Laboratory QA samples will be analyzed in accordance with method-specific and program- specific<br />

protocols. These samples will include method blanks, LCS, matrix spikes and matrix spike duplicate<br />

(MS/MSD), and laboratory duplicates.<br />

Method blank samples are generated within the laboratory and used to assess contamination resulting<br />

from sample preparation and extraction procedures. Method duplicate samples are analyzed for<br />

inorganic methods to confirm sampling and analytical reproducibility. MS/MSD samples provide<br />

information about effects of the sample matrix on sample digestion and analysis. One MS/MSD will be<br />

Kirtland AFB<br />

Quality Assurance Project Plan C-23 April 2004

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