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KIRTLAND AIR FORCE BASE ALBUQUERQUE, NEW MEXICO ...

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APPENDIX C<br />

10. DATA VALIDATION, REDUCTION, AND REPORTING<br />

10.1 Data Validation<br />

The following section describes the procedures pertaining to data validation of both the field and the<br />

analytical laboratory data.<br />

10.1.1 Laboratory Data<br />

Laboratory data will be validated according to procedures outlined in the current EPA National<br />

Functional Guidelines for Organic Data Review, and EPA National Functional Guidelines for Inorganic<br />

Data Review (Functional Guidelines), EPA Region 6 and NMED guidance, and USACE and USAF<br />

requirements as appropriate. For analytical methods with nonexistent data validation guidelines, SOPs<br />

will be developed prior to evaluation. Data validation procedures will be documented in the projectspecific<br />

QAPP.<br />

Criteria to be evaluated for organic analyses include, but are not limited to:<br />

C-O-C quality<br />

Holding times<br />

Instrument calibration<br />

Blanks (including method, trip, ambient air, and equipment)<br />

Method reporting limits<br />

Laboratory corrective actions<br />

Surrogate monitoring compound recovery<br />

MS/MSD recovery<br />

Internal standard performance<br />

Data completeness<br />

Results, which do not meet acceptance criteria as provided in the Functional Guidelines, or project<br />

requirements will be qualified with the appropriate data flags.<br />

Criteria to be evaluated for inorganic analyses include:<br />

C-O-C quality<br />

Holding times<br />

Instrument calibration<br />

Kirtland AFB<br />

Quality Assurance Project Plan C-47 April 2004

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