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KIRTLAND AIR FORCE BASE ALBUQUERQUE, NEW MEXICO ...

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APPENDIX C<br />

Blanks (including method, calibration, and equipment)<br />

Method reporting limits<br />

Laboratory corrective actions<br />

Inductively coupled plasma (ICP) interference check,<br />

MS/MSD recovery<br />

LCS recovery<br />

Review of furnace analytical spike recovery or method of standard additions<br />

Serial dilution analyses<br />

Data completeness<br />

Results which do not meet acceptable criteria as provided in the Functional Guidelines or SOPs will be<br />

qualified with the appropriate qualifier code.<br />

Following the validation procedure, a summary report will be prepared which briefly outlines the<br />

rationale for and the significance of all qualifier codes applied to the analytical data. The following data<br />

validation qualifiers may be added to the data based upon the merit of the QC results associated with the<br />

data:<br />

U<br />

R<br />

J<br />

UJ<br />

Value is a non-detect as reported by the laboratory, or has been qualified as a false<br />

positive based on contamination found in associated blanks.<br />

Value is considered to be unreliable and is unusable due to significant noncompliance<br />

with associated QC criteria.<br />

Positive value is considered to be an estimate based on associated QC parameter<br />

exceedances.<br />

Detection limit is considered to be estimated based on associated QC parameter<br />

exceedances.<br />

10.1.2 Field Records<br />

Field documentation will ensure sample integrity and provide sufficient technical information to recreate<br />

each field event. All field data will be reviewed to ensure that:<br />

Proper field procedures are implemented<br />

Appropriate documentation is available for each activity<br />

Field instruments are calibrated as required<br />

Required number and type of field QC samples are collected<br />

Kirtland AFB<br />

Quality Assurance Project Plan C-48 April 2004

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