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KIRTLAND AIR FORCE BASE ALBUQUERQUE, NEW MEXICO ...

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APPENDIX D<br />

Upon completion of the field data review, the qualifiers attesting to the usability of the data will be<br />

assigned and transmitted to the database manager for entry into the EDMS. All reports and field records<br />

will be submitted to Records Management personnel for archival in the project files (Records<br />

Management Task).<br />

4.2.2 Analytical Data Validation<br />

Depending upon project requirements, different levels of analytical data validation may be specified. In<br />

general, analytical data will be validated to ensure that:<br />

The laboratory procedures conform to the prescribed analytical method<br />

The samples are analyzed within the method-specified holding times<br />

All QC samples are analyzed at the required frequency<br />

The QC criteria are within specified limits<br />

The instrument used is calibrated as required by the method<br />

Appropriate detection limits are achieved<br />

No numerical/transcription errors are present<br />

The data package is complete and required documentation is provided<br />

At a minimum, the following items will be reviewed, as applicable, to validate the data depending on<br />

project requirements:<br />

Sample holding times<br />

Instrument performance<br />

Calibration (initial and continuing)<br />

Blanks<br />

Surrogate recovery<br />

Internal standard recovery<br />

Matrix spike/matrix spike duplicate<br />

Field and laboratory duplicate precision<br />

Laboratory control sample<br />

Interference check sample<br />

Inductively-coupled plasma serial dilution results<br />

Kirtland AFB<br />

Data Management Plan D-20 April 2004

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