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Thixoforming : Semi-solid Metal Processing

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Figure 6.36 Experimental setup, T-shaped die.<br />

6.2 Numerical Modelling of Flow Behaviourj203<br />

Model Parameter Determination and Adjustment The model parameters m, n, t0, k<br />

and C (see Equation 6.1) were determined on the basis of the step change shear rate<br />

experiments and also shear rate ramp experiments at a reference <strong>solid</strong> content f S,ref. of<br />

52% The rheological experiments led to reliable results for the yield stress t0, the flow<br />

exponent n and the consistency coefficient k. These model parameters are related to<br />

steady-state conditions. The determination of the isostructure flow exponent m and<br />

the rate constant c (Equation 6.5), which describe the transient behaviour of the<br />

material, suffers from a slight uncertainty.<br />

Ordinary die filling processes do not last longer than approximately 0.5 s. During<br />

this time, the semi-<strong>solid</strong> alloy undergoes a lot of shear rate changes and jumps. Hence<br />

the time span for a shear rate jump is in the range of milliseconds. So far there is no<br />

possibility of acquiring viscosity values at these time scales with conventional<br />

rheometers. A further problem arises from the permeability coefficient kP used in<br />

the two-phase model.<br />

In order to overcome these problems, a special approach of parameter adjustment<br />

has been developed (Figure 6.37). The aim is to achieve congruence between<br />

numerical and experimental results. The filling experiments are carried out under<br />

isothermal conditions. Varying the filling velocity and the initial <strong>solid</strong> fraction of the<br />

metallic suspension leads to different filling pressures, flow patterns and spatial<br />

distributions of <strong>solid</strong> content. The simulation starts with a set of parameters<br />

determined on the basis of the rheological experiments performed and a first guess<br />

of the permeability coefficient. As long as no congruence of the flow front contour, the<br />

<strong>solid</strong> fraction distribution and the filling pressure is achieved, a new simulation with<br />

modified flow exponent m, rate constant c and permeability coefficient k P is carried<br />

out.<br />

Two-phase Simulation Using the obtained set of material parameters, the T-shaped<br />

die-filling experiment described above was simulated using the two-phase model<br />

implemented into the solving algorithm PETERA. In order to show that the flow is<br />

mainly influenced by segregation effects, one-phase simulations considering yield

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