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Thixoforming : Semi-solid Metal Processing

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Table 11.5 Tool characteristics of self-heating thixoextrusion tool.<br />

Container<br />

Material Al2O3, 99.7%<br />

Inner diameter [mm] 85<br />

Outer diameter [mm] 125<br />

Cross-sectional area [mm 2 ] 5674.5<br />

Wall thickness [mm] 20<br />

Height [mm] 250<br />

Die<br />

Material Si 3N 4<br />

Cross-sectional area [mm 2 ] 301.8<br />

Extrusion channel length [mm] 300<br />

Feeding angle [ ] 11.3<br />

Extrusion ratio 18.8<br />

required. With an inductive heating device, the billets were heated with time–power<br />

strategies into the semi-<strong>solid</strong> state with maximum power first, followed by homogenization<br />

phases to ensure a homogeneous temperature distribution in the billet<br />

(Figure 11.13). During heating, the billet was prevented from oxidation by the inert<br />

gas argon. Thermocouples measured the temperature development in the billet.<br />

With the three-stage strategy, a final temperature of 1270 C was realized. This<br />

corresponds to a liquid fraction of approximately 40%, according to differential<br />

thermal analysis as described in Chapter 3. With this strategy, the billets were<br />

homogeneously semi-<strong>solid</strong> but still dimensionally stable and subsequently extruded.<br />

After the heating procedure, the billets were manipulated within 7 s to the<br />

extrusion tool and subsequently extruded by the 6.3 MN SMS Meer open die forging<br />

press.<br />

Figure 11.11 Si3N4 thixoextrusion die for upscaled extrusion tests.<br />

11.4 Isothermal Thixoextrusionj425

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