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Thixoforming : Semi-solid Metal Processing

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428j 11 Thixoextrusion<br />

impacts. Extensive finite element method simulations of temperature profiles and<br />

process-induced stresses are essential for defect-free long-term application of<br />

ceramic dies in order to benefit from the excellent corrosion and wear resistance<br />

of these materials.<br />

This also includes effective control of the <strong>solid</strong>ification step during thixoextrusion.<br />

A stable and preferably flat <strong>solid</strong>ification front is required in order to retain the shape<br />

of extruded bars and minimize residual porosity by <strong>solid</strong>ification at least under low<br />

pressure. Potential solutions include providing guide rollers, as depicted in the tool<br />

concept scheme in Figure 11.2, not available in the experiments reported here, on the<br />

target to stabilize the as-formed bars until <strong>solid</strong>ification is fully accomplished.<br />

Alternatively, a secondary, non-isothermal die exhibiting a defined temperature<br />

profile adjusted to the work alloy and extrusion velocity may be provided below the<br />

isothermal forming die to control <strong>solid</strong>ification. In the latter case, independently<br />

controlled heating cores and a segmented die construction using tailored die<br />

materials are essential.<br />

In this respect, the tool setups and experimental results obtained hitherto merely<br />

mark the beginning of possibilities for the isothermal semi-<strong>solid</strong> processing of highmelting<br />

alloys. Similarly to other complex, but established, metal forming processes<br />

relying on accurate <strong>solid</strong>ification control such as continuous casting and thin strip<br />

casting, the transfer of laboratory-scale results to a table process on an industrial scale<br />

remains a challenging task.<br />

11.5<br />

Non-isothermal Thixoextrusion<br />

11.5.1<br />

Experimental Strategy, Tools and Process Parameters<br />

The non-isothermal thixoextrusion experiments were carried out on the SMS Meer<br />

open die forging press. Due to the press design, the extrusion experiments were<br />

carried out in a vertical direction. The lowest press velocity possible was 10 mm s 1 .<br />

For this series of experiments, the version of direct extrusion was chosen. The punch<br />

moved in the same direction as the extruded bar. The dimensions of the container<br />

(inner diameter 85 mm) were based on the calculations of the maximum hydrostatic<br />

pressure. The extrusion tool was designed in a modular way (Figure 11.16a). The<br />

forming die holder could be opened to remove the forming die, the discard and the<br />

dummy plate afterwards. The tool was designed to extrude billets with a diameter of<br />

76 mm and a height of 100 mm (Figure 11.16b).<br />

The extrusion tool was actively heated to 300 C whereas the forming die was<br />

heated to 600 C in an external furnace to prevent early <strong>solid</strong>ification of the billet<br />

material after coming in contact with the forming die. The forming die was inserted<br />

in the container before the extrusion process. This allowed the height of the forming<br />

die and also the geometry of the extrusion channel to be changed but prohibited<br />

integration of an active cooling system. Additional cooling tube was not installed

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