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Proceedings of SerbiaTrib '13

Proceedings of SerbiaTrib '13

Proceedings of SerbiaTrib '13

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comparison with the synthetic reinforcements suchas silicon carbide (SiC) and alumina (Al 2 O 3 ) [16].The properties achieved with the sole utilization <strong>of</strong>these cheaper source reinforcements have beenreported to be lower than that <strong>of</strong> the syntheticreinforced but with promise for use in semistructuraland thermal management applications[17]. The use <strong>of</strong> hybrid reinforcements utilizingSiC/Al 2 O 3 and agro waste ashes as a means <strong>of</strong>improving the properties <strong>of</strong> AMCs has attractedinterest recently with very encouraging resultsobtained [18-19].The present work is aimed at investigating theinfluence <strong>of</strong> the weight ratios <strong>of</strong> rice husk ash andsilicon carbide on the mechanical behaviourAluminium matrix hybrid composites having variedweight percent <strong>of</strong> both reinforcements. Themotivation for this work is to establish optimumRHA/SiC weight ratios required to achieveoptimized performance <strong>of</strong> low cost AMCs developedwith the use <strong>of</strong> rice husk. Literatures on the use <strong>of</strong>synthetic/agrowaste hybrid reinforcements forAMCs development are still very limited and there iscurrently none that the authors are aware <strong>of</strong> thatdiscusses the use <strong>of</strong> RHA and SiC as hybridcomposites in Al-Mg-Si alloy matrix.2. MATERIALS AND METHOD2.1 MaterialsAl-Mg-Si alloy billets with chemicalcomposition determined using spark spectrometricanalysis (Table 1) was selected as Aluminiummatrix for this investigation.Table 1. Elemental composition <strong>of</strong> Al-Mg-Si alloy.Elementwt%Si 0.4002Fe 0.2201Cu 0.008Mn 0.0109Mg 0.3961Cr 0.0302Zn 0.0202Ti 0.0125Ni 0.0101Sn 0.0021Pb 0.0011Ca 0.0015Cd 0.0003Na 0.0009V 0.0027Al 98.88For the hybrid reinforcing phases, siliconcarbide (SiC) and rice husk ash (RHA) wereselected. The silicon carbide procured was <strong>of</strong> highchemical purity with average particle size <strong>of</strong> 28µmwhile rice husks utilized for the processing <strong>of</strong> ricehusk ash was obtained from Igbemo-Ekiti, EkitiState (a rice producing community in south westernNigeria). Magnesium for improving wettabilitybetween the Al-Mg-Si alloy and the reinforcementswas also procured.2.2 Preparation <strong>of</strong> Rice Husk AshThe procedure adopted is in accordance withAlaneme et al [16]. It involves the use <strong>of</strong> a simplemetallic drum with perforations as burner for therice husk. Dry rice husks placed inside the drumwas ignited with the use <strong>of</strong> charcoal. The husk wasallowed to burn completely and the ashes removed24 hours later. The ash was then heat-treated at atemperature <strong>of</strong> 650 o C for 180 minutes to reduce itscarbonaceous and volatile constituents. Sieving <strong>of</strong>the bamboo leaf ash was then performed using asieve shaker to obtain ashes with mesh size under50µm. The chemical composition <strong>of</strong> the rice huskash from this process is presented in Table 2.Table 2. Chemical Composition <strong>of</strong> the Rice Husk AshCompound/Element (constituent) weight PercentSilica (SiO 2 ) 91.59Carbon, C 4.8Calcium oxide CaO 1.58Magnesium oxide, MgO 0.53Potassium oxide, K 2 O 0.39Haematite, Fe 2 O 3 0.21Sodium, NatraceTitanium oxide, TiO 2 0.202.3 Composites ProductionTwo step stir casting process was utilized toproduce the composites [20]. The process startedwith the determination <strong>of</strong> the quantities <strong>of</strong> rice huskash (RHA) and silicon carbide (SiC) required toproduce 5, 7.5, and 10 wt% reinforcementconsisting <strong>of</strong> RHA and SiC in weight ratios 0:1,1:3, 1:1, 3:1, and 1:0 respectively (which amountsto 0, 25, 50, 75, and 100% RHA in thereinforcement phase). The rice husk ash and siliconcarbide particles were initially preheated separatelyat a temperature <strong>of</strong> 250 o C to eliminate dampnessand improve wettability with the molten Al-Mg-Sialloy. The Al-Mg-Si alloy billets were charged intoa gas-fired crucible furnace (fitted with atemperature probe), and heated to a temperature <strong>of</strong>750 o C ± 30 o C (above the liquidus temperature <strong>of</strong>the alloy) to ensure the alloy melts completely. Theliquid alloy was then cooled in the furnace to asemi solid state at a temperature <strong>of</strong> about 600 o C.The preheated rice husk ash and SiC particles alongwith 0.1 wt% magnesium were then charged into13 th International Conference on Tribology – Serbiatrib’13 161

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