11.07.2015 Views

Proceedings of SerbiaTrib '13

Proceedings of SerbiaTrib '13

Proceedings of SerbiaTrib '13

SHOW MORE
SHOW LESS
  • No tags were found...

You also want an ePaper? Increase the reach of your titles

YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.

It has already been mentioned that t four factors,each at three levels, have been selected to conductthe abrasiontest. Table 3 indicates the said factor –level combinations and corresponding specific wearrate data which is obtained fromthe followingformula [11]:mW sFL,where, W s = specific wear rate (mmm 3 /Nm)Δm = mass loss recorded gravimetricallyy(gm)ρ = specific gravity <strong>of</strong> EPDM (gm/cm 3 )F = the normalload on the job (N)and, L = overall sliding distance(m)The worn surface morphology had been studiedfor each sample immediately after the abrasionusing a scanning electron microscope (SEM: JEOL,JSM-6360, model 75 82) to see thesmallest detail<strong>of</strong> the pattern abrasion in the range <strong>of</strong> 4 – 5 nm (4 –5 millionths <strong>of</strong> a millimeter). Thetest had beenconducted immediately after the experiment, thoughit is reported by Pandey et.al. [14] that in theirexperimentsfracture mode did not change withinn 72hours <strong>of</strong> storage before conducting SEM studiess andcoating etc. The worn surfaces had been coated witha very thinlayer <strong>of</strong> palladium (Pd) using ionsputtering machine (Auto Fine Coater: JEOL, JFC-to1600) prior to SEM studies. It is not out <strong>of</strong> placemention here that ioncoating is done on non-etc.)conducting specimen (like biological specimento be analyzed in SEM for quick and highlyefficient results. This is done mainly to preventcharging <strong>of</strong>electrons atthe sample[15]. For somesamples energy dispersive X-ray spectroscopy(EDAX) had also beendone in conjunction withSEM to find out thepercentages <strong>of</strong> differentelements inthe sample. Elemental mapping withEDAX is helpful to get insight into the chemicalchanges onthe surface and sub-surface <strong>of</strong> thesample[16].As no chemical reactionis taking placein the present case hence EDAX hass not done for allthe specimens.Figure 6 shows some typical pattern abrasion <strong>of</strong>EPDM as obtained fromSEM studies. In figure 6(b)a chunk <strong>of</strong> rubber agglomerate hass been separatedleaving behind a groove (chunkingand grooving).Figure 6(c) reveals the ridge formation whichsupports theconcept <strong>of</strong>rubber wear by the process<strong>of</strong> plowing.(a)(b)(c)Figure 6. Worn W surface morphology <strong>of</strong> EPDMcorrespondingg to trial no.1 (×200), 2 (×1000) and 6(×2000) as obtained from SEM studies.The graph <strong>of</strong> o the average specific wear rate isshown in Figuree 7.13 th International Conference on Tribology – Serbiatrib’133777

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!