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Proceedings of SerbiaTrib '13

Proceedings of SerbiaTrib '13

Proceedings of SerbiaTrib '13

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Figure 1. Transverse and longitudinal cross-section <strong>of</strong>hardened specimenThe specimen test section had a cylindrical form<strong>of</strong> dimension 25 × 10 mm (diameter × height).Specimens with porosity <strong>of</strong> about 19% to 50%,were prepared by laser technique, followed byhardening at T ∈ [1000, 1400] °C and v ∈ [2, 5]mm/s. First, we changed two parameters <strong>of</strong> therobot laser cell: speed v ∈ [2, 5] mm/s with steps <strong>of</strong>1 mm/s and temperature T ∈ [1000, 1400] °C insteps <strong>of</strong> 100 °C (Fig. 2). Secondly, we repeated theprocess (Fig. 3). In addition, we hardened thespecimens again with equal parameters <strong>of</strong> the robotlaser cell. The microstructure <strong>of</strong> the specimens wasobserved with a field emission scanning electronmicroscope (JSM-7600F, JEOL Ltd.). An irregularsurface texture was observed with a few breaks,which are represented by black islands (Fig. 4). Fig.5 presents the boundary between the hardened andnon-hardened material.Figure 2. Robot laser hardening with differenttemperature and speedFigure 3. Repeated process <strong>of</strong> robot laser hardeningFigure 4. SEM picture <strong>of</strong> robot laser re-hardenedspecimenFigure 5. The boundary between work-hardened andnon-hardened materialWe used the method <strong>of</strong> determining the porosityfrom SEM images <strong>of</strong> the microstructure. It isknown that in a homogenously porous material thearea <strong>of</strong> pores is equal to the volume <strong>of</strong> pores inspecimens. The SEM pictures were converted tobinary images (Fig. 6), from which we calculatedthe area <strong>of</strong> pores <strong>of</strong> all pictures using the ImageJprogram (ImageJ is a public domain, Java-basedimage processing program developed at theNational Institutes <strong>of</strong> Health). The area <strong>of</strong> pores oneach picture <strong>of</strong> the material was calculated and thenthe arithmetic mean and standard deviation <strong>of</strong>porosity were determined. To analyze he possibility<strong>of</strong> the application <strong>of</strong> fractal analysis to the heattreatedsurface, we examined the relation betweenthe surface porosity and fractal dimensionsdepending on various parameters <strong>of</strong> the robot lasercell. In fractal geometry, the key parameter is thefractal dimension D. The relationship between thefractal dimension D, volume V and length L, can beindicated as follows:V~L D (1)356 13 th International Conference on Tribology – Serbiatrib’13

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