stroke engines by physic-chemical methods in orderto evaluate possibilities <strong>of</strong> engine conditionmonitoring by oil analysis. This part presents theresults <strong>of</strong> experimental research <strong>of</strong> physic-chemicalcharacteristics <strong>of</strong> engines oil which was sampledfrom engines <strong>of</strong> PUCH 300GD, Pinzgauer 710 andIKARBUS IK 104P vehicles [9], [10].The research was carried out in two vehiclesPUCH 300GD (PUCH-1, PUCH-2), two vehiclesPINZGAUER 710M (PINZ-1, PINZ-2) and twovehicles IKARBUS IK 104P (IK104P-1, IK104P-2).The research was conducted through periodicsampling oil from engine vehicles listed above.Apart from the fresh oil (“zero” sample), samplesare taken after 1.000 km, 2.000 km, 3.000 km,4.000 km and 5.000 km for vehicles.The physical-chemical characteristics <strong>of</strong> oil inaccordance with standard methods are examined,shown in table 1.Table 1. Implemented tests and methods for examiningthe physic-chemical characteristics <strong>of</strong> oilCharacteristicMethodKinematic viscosity, mm 2 /s SRPS B.H8.022Viscosity IndexSRPS B.H8.024Flash Point (C) ISO 2592, ASTM D 92Pour Point (C) ISO 3016Water Content, mas.% ASTM D 95Total Base Number (TBN),mgKOH/gASTM D 2896Insoluble substances inpentane, %ASTM D 893Insoluble substances inbenzene, %ASTM D 4055Fe Content, %ASSCu Content, %ASSThe analysis was done on the fresh (new) oilsand oils that are used in the engines <strong>of</strong> vehicles.During the sampling <strong>of</strong> oil choice <strong>of</strong> the samplingwere conducted carefully according to the actual oilusage, which enabled each sample as representativeone.The wear mechanism <strong>of</strong> a tribologicallubrication system consists in the wear <strong>of</strong> contactsurfaces, and lubricant consumption. If there iswear <strong>of</strong> the contact surfaces, there are wearparticles present.Regardless <strong>of</strong> the availability <strong>of</strong> numerousmethods for diagnosing the physic-chemicalchanges <strong>of</strong> lubricants, in order to create a truepicture <strong>of</strong> the condition <strong>of</strong> lubricants from the usersystem, it is <strong>of</strong> importance to satisfy theprecondition <strong>of</strong> the possibility to obtain arepresentative sample. That is why it is extremelyimportant to take the sample in a proper way.Allowable values <strong>of</strong> deviation limits <strong>of</strong>individual characteristics <strong>of</strong> the oil are conditionedby the type <strong>of</strong> oil, working conditions and internalrecommendations <strong>of</strong> the manufacturer <strong>of</strong> lubricantsand users. Limited value characteristics <strong>of</strong> oils thatcondition the change <strong>of</strong> oil charging from engineare given in table 2. They represent the criteria forthe change <strong>of</strong> oil charge. Deviation <strong>of</strong> only onesource changes characteristics <strong>of</strong> oil charge, nomatter <strong>of</strong> what a characteristic is about.Table 2. Allowed values deviation <strong>of</strong> physico-chemicalcharacteristics <strong>of</strong> new and used oilPhysical-chemicalcharacteristics oil andproducts wearViscosity at 40C and100C, mm 2 /sMaximum allowedvariationMotor oil20%Viscosity Index, % 5 %Total Base Number (TBN),mg KOH/gr The fall to 50%Flash Point, C 20 %Water Content, % 0,2 %Products wear – Content Fe,ppm(μg/gr)100 ppmProducts wear – Content Cu,ppm(μg/gr)50 ppmUsed engine oil in examined vehicles are shownin table 3. Characteristics <strong>of</strong> zero samples <strong>of</strong> motoroil are shown in table 4, and the results used oilsamples in table 5.Table 3. Used engine oil in examined vehicles [9]Engine oil from engine <strong>of</strong> PUCH 300 GD vehiclesSAEclassificationAPIclassificationManufacturerFAMSAE 15W-40 API SG/CEKrusevacEngine oil from engine <strong>of</strong> PINZGAUER 710 M vehiclesSAEclassificationAPIclassificationManufacturerGALAXSAE 30/S3 -BeogradEngine oil from engine <strong>of</strong> IKARBUS 104 P vehiclesSAEclassificationSAE 15W-40APIclassificationAPI SG/CEManufacturerFAMKrusevacThe viscosity index is an empirical numberwhich shows how the viscosity <strong>of</strong> some oilschanges by increasing or reducing the temperature.High viscosity index shows relatively smalltendency <strong>of</strong> viscosity to change upon influence <strong>of</strong>certain temperature, as oppose <strong>of</strong> low viscosityindex which shows greater viscosity change withtemperature.242 13 th International Conference on Tribology – Serbiatrib’13
Table 4. Results <strong>of</strong> zero samples <strong>of</strong> oil from the engine[9]Type <strong>of</strong> motor oilCharacteristic FAMSAE 15W-40GalaxSAE 30/S3Color 3,0 3,0Density, gr/cm 3 0,881 0,902Viscosity at 40C,mm 2 /s104,81 104,63Viscosity at100C, mm 2 /s14,12 11,67Viscosity Index ─ ─Flash Point, C 230 240TBN,mg KOH/g10,5 9,8Table 5. The results <strong>of</strong> testing samples <strong>of</strong> used oil fromengines examined vehicles [9]SamplePUCH PUCH IK104 IK104 PINZ PINZ–1 –2 –1 –2 –1 –20 14,1 14,1 14,1 14,1 11,6 11,61 14,6 14,2 13,7 13,6 10,9 10,52 15,4 15,0 12,8 13,5 10,3 10,43 16,0 15,6 12,4 13,2 9,96 10,14 16,6 16,1 12,3 12,9 9,3 9,65 17,5 17,0 12,2 12,6 8,7 9,00 104,8 104,8 104,8 104,8 104,6 104,61 111,0 110,4 96,9 104,4 100,4 100,92 113,5 111,8 96,2 101,9 94,4 96,13 119,4 113,8 92,3 97,1 86,3 88,64 126,4 115,9 90,8 94,8 79,1 82,25 132,7 127,5 90,2 93,1 75,9 76,9Viscosity at100C, mm 2 /sViscosity at40C, mm 2 /sViscosityIndexFlashPoint,CTBN,mgKOH/gFe Content(ppm)Cu Content(ppm)0 135 135 135 135 100 1001 129 131 132 133 96 972 122 126 130 131 93 953 119 123 125 127 89 914 116 120 122 124 84 875 112 115 119 121 82 840 230 230 230 230 240 2401 220 215 217 212 196 1932 208 210 214 210 186 1773 205 204 213 202 168 1594 197 202 210 193 154 1435 192 188 189 184 136 1280 10,5 10,5 10,5 10,5 9,8 9,81 9,1 9,4 8,8 8,1 9,6 9,42 7,2 8,9 8,7 7,7 9,1 8,43 6,5 8,7 8,4 7,2 8,3 7,84 6,1 8,1 7,9 6,8 7,6 6,65 5,2 7,6 7,3 6,4 7,1 6,21 98,4 27,4 30,1 20,5 19 17,92 123 59,8 32,5 46,3 19,8 40,93 137,1 71,2 35,6 57,6 38,3 86,74 149,4 71,4 37,5 62,8 54,3 132,85 165,3 86,8 38,5 69,6 105,4 2611 4,9 2 1,5 3,2 3,5 3,32 5,9 3,4 1,9 5,1 4,1 3,83 6,7 3,7 3,2 6,3 5,3 64 7,3 3,9 4,4 7,7 6,9 8,15 7,9 5,4 4,9 9,1 8,7 9,7During the exploitation it is desired that theviscosity changes as lesser as possible with thechange <strong>of</strong> temperature. If during work temperaturemodes are changeable and cause major changes <strong>of</strong>viscosity that may cause disruptions in thefunctioning <strong>of</strong> the system, which is a manifestation<strong>of</strong> increased friction, wear and damage.Change <strong>of</strong> engine oil Viscosity Index is shownin the figure 1. The decrease in the Viscosity Indexoil is evident for all vehicles, exceeding the limit <strong>of</strong>5 % (table 2).Viscosity Index1401301201101009080Max allowed decrease 5 %= 128,25 (SAE 15W-40)Max allowed decrease 5 %= 95 (SAE 30)0 1000 2000 3000 4000 5000Crossed kilometers, kmIndex viscosity <strong>of</strong> "0" sample:135 (SAE 15W-40)PUCH−1PUCH−2PINZ−1PINZ−2IK104P−1IK104P−2Figure 1. The change <strong>of</strong> Viscosity Index [9]The most important engine oils characteristic isthe viscosity defined as a measure <strong>of</strong> inner frictionwhich works as a resistance to the change <strong>of</strong>molecule positions in fluid flows when they areunder the impact <strong>of</strong> shear force, or in other words,it is the resistance <strong>of</strong> fluid particles to shear.The viscosity is a changeable category and itdepends on the change <strong>of</strong> temperature and pressure.A higher temperature reduces the viscosity andmakes a fluid thinner.Multigrade engine oils among numerousadditives always contain also viscosity indeximprovers. These additives are special types <strong>of</strong>polymers, which in small concentrationsignificantly improve engine oils rheologicalproperties, especially viscosity and viscosity index.However, during engine oils utilization,degradation <strong>of</strong> viscosity index improvers i.e. Breakdown <strong>of</strong> polymeric molecules occurs. It results inreduction <strong>of</strong> their molecular weight what leads toviscosity loss and oil film thickness decrease,which causes undesirable phenomena <strong>of</strong> frictionand wear.Reasons for the increase <strong>of</strong> viscosity lubricantsare as follows: oxidation <strong>of</strong> lubricants, cavitationsdue to foaming lubricants, dissolution <strong>of</strong> lubricantswith water, pouring and charging system viscosityfat greater than recommended and contamination <strong>of</strong>solid particles and products wear lubricants.The reasons for the reduction <strong>of</strong> lubricantsviscosity are: lubricants contamination <strong>of</strong> fuel (formotor oil), shearing additive for reclamationviscosity, drop point <strong>of</strong> flash, grinding molecules,lubricants contamination without solubility withwater, pouring and charging system viscosity lessfat than recommended, and the impact <strong>of</strong> liquid13 th International Conference on Tribology – Serbiatrib’13 243
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SerbianTribologySocietyFacultyofEng
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Serbian Tribology SocietyUniversity
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Supported byMinistry of Education,
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PrefaceThe International Conference
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ContentsPlenary Lectures1. THE GREE
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27. WEAR CHARACTERISTICS OF HYBRID
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Tribometry57. PRELIMINARY STUDY ON
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Plenary Lectures13 th International
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Figure 4. Diagram of the height and
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Realization of the approach is base
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edge without chamfer and smaller ra
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Figure 7. Accumulated tool life in
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Figure 13. Calculated and measured
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Friction deformation of the bronze
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engine cylinders of 2-cylinder-twot
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Table 1: Chemical composition of sa
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Table 4: Comparative wear-resistanc
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- measuring of coating thickness h
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Figure 5. Functional scheme of the
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Table 2. Test results for massive w
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knowledge transfer in the field ofm
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Table 1. Parameters of the electroc
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Figure 6. Wear resistance by linear
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coatings and observed their good we
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c)a)Figure 2: SEM images and micros
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Room temperature 300°CNi/µSiCNiNi
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COF [-] COF [-]Fig.9: COF graphs at
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about 260 nm is related to isolated
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contact’s conformity [18] they ob
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In order to calculate the metallic
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microscopic inspection of the Rp3 s
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otating plate. The shaft passes thr
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similar trends of variation are obs
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smooth, gear fiber-mild steel rough
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[2] Tabor, D.: “Friction and wear
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(10, 50 and 100 N) against surface
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[9] B.R. Gligorijevic, A. Vencl, B.
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dielectric properties, high resista
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parameter, Sv, was slightly influen
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dependence of roughness height and
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Polyethylenes with a molecular weig
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[9] K.S. Kanaga Karuppiah, A.L. Bru
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MgCO3•CaCO3 (13% Mg), and carnall
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fully compatible with MRI/MSCT imag
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5. CONCLUSIONThe magnesium alloys a
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Zinc dialkyldithiophosphate (ZDDP)
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C- Lower deposits with NPNA on comb
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films. Carraro et al. [10] examined
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PlateCount No.Critical Load ( N)120
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solid melt of ZA27 alloy using mech
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SiC particles are uniformly distrib
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in number of micro-cracks and clust
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PBT has the average values of the f
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mechanical pressure and thermal loa
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3. EXPERIMENTAL RESULTSTaking into
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[12] L. Blunt De, X. Jiang: Advance
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2. EXPERIMENTALTESTING2.1 MaterialT
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figure 3a it could be seen that the
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and lubrication is done so that the
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5. CONCLUSIONFigure 11. The accumul
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esistance was found for composite c
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onze, which is embedded within the
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The test contact pair meets the req
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complete. The SEM analysis maycontr
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tg( ) tg 100, [%] (2)tgwhere are:
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corresponding to the maximum value
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electrostatics [17]. Due to the fle
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250nm size have been observed, acco
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ETH Zurich, Switzerland, where all
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comparison with the synthetic reinf
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3. RESULTS AND DISCUSSION3.1 Micros
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(a)(b)Figure 4. Showing (a) variati
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composites. But the composite compo
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coated and uncoated region after ad
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has been measured between the top s
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Fig. 9 shows the wear track obtaine
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Mica samples preparationFor the ads
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According to the AFM results in fig
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[21] B. G. Sharma et al.: Character
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chemical vapor deposition method wi
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analysis (a) and an approximate che
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Table 3. Friction coefficients of s
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Figure 2. Structure of the machinin
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3. ANALYSIS OF RESULTSThe results o
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Figure 15. Surface roughness regard
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From the analysis of the diagram it
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comparison from economic, energy co
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Advantages and disadvantages of tra
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The information provided by footwea
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Force (N)5,554,543,532,521,510,50Ex
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additives, that had been, until rec
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Figure 1. Test results for samples
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Table 7. Test results of oil sample
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Input parameters- Current intensity
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edge formed into a thin line. At th
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Lower values of current are not res
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Table 1. Chemical composition of si
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flowable at high temperatures and v
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holes (pits) emerge in the shape of
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[4] W. Schatt, K-P. Wieters, Pulver
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assumption allows us to use, instea
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where P is the load, a - radius of
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determination (total running in tim
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μm, compared with Figure 17, wich
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Especially when the chain transfer
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is obvious that this isa so-calledw
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winches. The authors are inclined t
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find parameters of robot laser hard
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each of which is measured by the le
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Fractal dimensions were determined
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Figure 3. Modified force acting sch
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0.25Lubricant: L3DC 04Friction coef
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nanocomposites. The influence of fi
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4. RESULTS AND DISCUSSION4.1 Morpho
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Figure 6. Loading and unloadin vers
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3 8 12 1 4 2 4
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The material after qualifying the r
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It has already been mentioned that
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Degradation & Stability, Vol. 69, N
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conformance to researchers’ requi
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This part is assembled of pneumatic
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matrixes describe the state of the
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values influence of themeasurement
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Figure 1. Friction stir weldinga -
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(t 2 t
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M fr / T [-] [-]10.90.80.70.60.50.4
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M fr / T [-]10.90.80.70.60.50.40.30
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experimentally determined that for
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4. DISCUSSIONAccording to the theor
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2.1 The life cycle of the reportThe
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Obviously the report is checked and
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uticaja na osnovu kompozita, a time
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5. ZAKLJUČCIStruktura tiksolivene
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dobijene različite karakteristike
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vizuelno, na dnevnoj svetlosti, pod
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LITERATURA[1] Зинченко В.
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Slika 1. Rotorni bager - glodar VII
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stvaraju sliku stanja i svoja zapa
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njihovih kotrljanih elemenata. Mere
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postupka i uticaja parametara depoz
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posledica različite raspodele mikr
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ZrO 2 Y 2 O 3 je takođe zbog oksid
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3.2 Pneumatska osetljivostOblast pr
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p mg (δ), koji je zbog malih struj
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PNEUMATIC PROBE HEAD SELECTION FOR
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1. Podsistem kopanja2. Podsistem pr
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Slika 3. Kriva habanjaNa tom dijagr
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Mjereni su parametri habanja i pril
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preše prevladavaju kombinirani uvj
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a) b)Slika 5. Karakteristična mikr
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varijantnih materijala u dostavnom
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Jovanović D. 414, 446KKaleicheva J
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CIP - Каталогизација