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BALTIC SEAENVIRONMENT PROCEEDINGS No. 59 - Helcom

BALTIC SEAENVIRONMENT PROCEEDINGS No. 59 - Helcom

BALTIC SEAENVIRONMENT PROCEEDINGS No. 59 - Helcom

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(Topping, 1992). Two principal components of QA are Quality con-<br />

trol and auality assessment. The former refers to measures which<br />

maintain analysis within an acceptable level of accuracy and<br />

precision. The latter refers to procedures adopted to provide<br />

documented evidence that the quality control is being achieved.<br />

In practice, Quality Assurance applies to all aspects of analy-<br />

tical investigation, and includes the following principal ele-<br />

ments:<br />

Provision and optimization of appropriate laboratory<br />

facilities and analytical equipment.<br />

Selection and training of staff for the analytical task<br />

in question.<br />

Establishment of definitive directions for appropriate<br />

collection, preservation, storage and transport proce-<br />

dures to maintain the integrity of samples prior to<br />

analysis.<br />

Use of suitable pre-treatment procedures, prior to<br />

analysis of samples, to prevent uncontrolled contamina-<br />

tion, and loss of the determinand, in the samples.<br />

Validation of appropriate analytical methods to ensure<br />

that measurements are of the required accuracy and pre-<br />

cision to meet the needs of the investigations.<br />

Conduct of regular intralaboratory checks on the accu-<br />

racy and precision of routine measurements, by the ana-<br />

lysis of appropriate reference materials, to assess<br />

whether the analytical methods are remaining under con-<br />

trol, and the documentation of the results on control<br />

charts.<br />

Participation in interlaboratory quality assessments to<br />

provide an independent assessment of the laboratory's<br />

capability of producing reliable measurements.<br />

The preparation, and use, of written laboratory proto-<br />

cols so that specific analytical data can be traced to<br />

the relevant samples, and vice versa.<br />

90

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