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O+.Part-IResults and DiscussionR 1NR 2NX eX = S, -C=C-IIIie, IIIiie, R 1 = R 2 = -(CH 2 ) 4 -, M + , m/e 219IIIiiie, IIIive, R 1 = CH 3 , R 2 = COOCH 3 , M + , m/e 237IIIve, IIIvie, R 1 = CH 3 , R 2 = COOC 2 H 5 , M + , m/e 252IIIviiie, R 1 = R 2 = CH 3 , M + , m/e 193IIIixe, IIIxe, R 1 = Ph, R 2 = H, M + , m/e 242IIIxie, R 1 = 4 - OCH 3 Ph, R 2 = H, M + , m/e 271IIIxiiie, IIIxive, R 1 = 4 - CH 3 Ph, R 2 = H, M + , m/e 256IIIxve, R 1 = 4 - BrPh, R 2 = H, M + , m/e 322IIIxviie, IIIxviiie, R 1 = 4 - ClPh, R 2 = H, M + , m/e 276IIIxixe, R 1 = Ph, R 2 = CH 3 , M + , m/e 255IIIxxe, IIIxxie, R 1 = R 2 = -(CH 2 ) 3 -, M + , m/e 205IIIxxiie, IIIxxiiie, R 1 = R 2 = -(CH 2 ) 5 -, M + , m/e 233IIIxxxive, R 1 = R 2 = -(-CH=CH - CH=CH-)-, M + , m/e 163IIIxxxia, R 1 = R 2 = -(-CH=C(OCH 3 )-C(OCH 3 )=CH-)-,R 3 = OCH 3 , M + , m/e 220O+R 1NHNSR 3NHNR 2 a-SHXX = S, -C=C-M-33IIIia, R 1 = R 2 = -(CH 2 ) 4 -, R 3 = H, M + , m/e 368IIIiia, R 1 = R 2 = -(CH 2 ) 4 -, R 3 = OCH 3 , M + , m/e 398IIIiiia, R 1 = CH 3 , R 2 = COOCH 3 , R 3 = H, M + , m/e 386IIIiva, R 1 = CH 3 , R 2 = COOCH 3 , R 3 = OCH 3 , M + , m/e 416IIIva, R 1 = CH 3 , R 2 = COOC 2 H 5 , R 3 = H, M + , m/e 400IIIvia, R 1 = CH 3 , R 2 = COOC 2 H 5 , R 3 = OCH 3 , M + , m/e 430IIIviiia, R 1 = R 2 = CH 3 , R 3 = OCH 3 , M + , m/e 372IIIixa, R 1 = Ph, R 2 = H, R 3 = H, M + , m/e 390IIIxa, R 1 = Ph, R 2 = H, R 3 = OCH 3 ,M + , m/e 420IIIxia, R 1 = 4 - OCH 3 Ph, R 2 = R 3 = H, M + , m/e 420R 1IIIxiia, R 1 = 4 - OCH 3 Ph, R 2 = H, R 3 = OCH 3 , M + , m/e 450IIIxiiia, R 1 = 4 - CH 3 Ph, R 2 = R 3 = H, M + , m/e 404IIIxiva, R 1 = 4 - CH 3 Ph, R 2 = H, R 3 = OCH 3 , M + , m/e 434IIIxva, R 1 = 4 - BrPh, R 2 = R 3 = H, M + , m/e 469IIIxvia, R 1 = 4 - BrPh, R 2 = H, R 3 = OCH 3 , M + , m/e 499 R 2IIIxviia, R 1 = 4 - ClPh, R 2 = R 3 = H, M + , m/e 424IIIxviiia, R 1 = 4 - ClPh, R 2 = H, R 3 = OCH 3 , M + , m/e 454IIIxixa, R 1 = Ph, R 2 = CH 3 , R 3 = H, M + , m/e 404IIIxxa, R 1 = R 2 = -(CH 2 ) 3 -, R 3 = H, M + , m/e 354IIIxxia, R 1 = R 2 = -(CH 2 ) 3 -, R 3 = OCH 3 , M + , m/e 384IIIxxiia, R 1 = R 2 = -(CH 2 ) 5 -, R 3 = H, M + , m/e 382IIIxxiiia, R 1 = R 2 = -(CH 2 ) 5 -, R 3 = OCH 3 , M + , m/e 412IIIxxxiva, R 1 = R 2 = -(-CH=CH - CH=CH-)-, R 3 = H, M + , m/e 308IIIxxxia, R 1 = R 2 = -(-CH=C(OCH 3 )-C(OCH 3 )=CH-)-, R 3 = OCH 3 ,M + , m/e 398-HSHNNXR 3R 1R 2 -XHNNONX = S, -C=C-NcNHSR 2NHR 1-COHNIIIic, R 1 = R 2 = -(CH 2 ) 4 -, R 3 = H, M + , m/e 307IIIiiic, R 1 = CH 3 , R 2 = COOCH 3 , R 3 = H, M + , m/e 325IIIvc, R 1 = CH 3 , R 2 = COOC 2 H 5 , M + , m/e 339IIIvic, R 1 = CH 3 , R 2 = COOC 2 H 5 , R 3 = OCH 3 , M + , m/e 369IIIviiic, R 1 = R 2 = CH 3 , R 3 = OCH 3 , M + , m/e 311IIIxic, R 1 = 4-OCH 3 Ph, R 2 = R 3 = H, M + , m/e 359IIIxiiic, R 1 = 4-CH 3 Ph, R 2 = R 3 = H, M + , m/e 343IIIxixc, R 1 = Ph, R 2 = CH 3 , R 3 = H, M + , m/e 343IIIxxc, R 1 = R 2 = -(CH 2 ) 3 -, R 3 = H, M + , m/e 393IIIxxiic, R 1 = R 2 = -(CH 2 ) 5 -, R 3 = H, M + , m/e 321.M-33-28NXONHR 3IIIid, IIIiiid, IIIvd, IIIixd, IIIxid, IIIxiiid, IIIxvd,IIIxviid, IIIxixd, IIIxxd, IIIxxiid, IIIxxxivd,R 3 = H, m/e 150IIIiid, IIIivd, IIIvid, IIIviiid, IIIxd, IIIxiid, IIIxivd,IIIxvid, IIIxviiid, IIIxxid, IIIxxiiid, IIIxxxid,R 3 = OCH 3 , m/e 180-R 3d.HNNR 3+.M-118 orM-148NN bNHIIIib, R 1 = R 2 = -(CH 2 ) 4 -, R 3 = H, M + , m/e 335IIIiib, R 1 = R 2 = -(CH 2 ) 4 -, R 3 = OCH 3 , M + , m/e 365IIIiiib, R 1 = CH 3 , R 2 = COOCH 3 , R 3 = H, M + , m/e 353IIIvb, R 1 = CH 3 , R 2 = COOC 2 H 5 , R 3 = H, M + , m/e 365IIIvib, R 1 = CH 3 , R 2 = COOC 2 H 5 , R 3 = OCH 3 , M + , m/e 397IIIviiib, R 1 = R 2 = CH 3 , R 3 = OCH 3 , M + , m/e 339IIIixb, R 1 = Ph, R 2 = H, R 3 = H, M + , m/e 357IIIxb, R 1 = Ph, R 2 = H, R 3 = OCH 3 , M + , m/e 387IIIxib, R 1 = 4 - OCH 3 Ph, R 2 = R 3 = H, M + , m/e 387IIIxiii, R 1 = 4 - CH 3 Ph, R 2 = R 3 = H, M + , m/e 371IIIxivb, R 1 = 4 - CH 3 Ph, R 2 = H, R 3 = OCH 3 , M + , m/e 401IIIxvb, R 1 = 4 - BrPh, R 2 = R 3 = H, M + , m/e 437IIIxviib, R 1 = 4 - ClPh, R 2 = R 3 = H, M + , m/e 391IIIxviiib, R 1 = 4 - ClPh, R 2 = H, R 3 = OCH 3 , M + , m/e 421IIIxixb, R 1 = Ph, R 2 = CH 3 , R 3 = H, M + , m/e 386IIIxxb, R 1 = R 2 = -(CH 2 ) 3 -, R 3 = H, M + , m/e 321IIIxxbi, R 1 = R 2 = -(CH 2 ) 3 -, R 3 = OCH 3 , M + , m/e 351IIIxxiib, R 1 = R 2 = -(CH 2 ) 5 -, R 3 = H, M + , m/e 349IIIxxiiib, R 1 = R 2 = -(CH 2 ) 5 -, R 3 = OCH 3 , M + , m/e 379IIIxxxivb, R 1 = R 2 = -(-CH=CH-CH=CH-)-, R 3 = H, M + , m/e 275IIIxxxib, R 1 = R 2 = -(-CH=C(OCH 3 )-C(OCH 3 )=CH-)-, R 3 = OCH 3 ,M + , m/e 365R 3R 2R 1XOfNX = S, -C=C-NHIIIif, R 1 = R 2 = -(CH 2 ) 4 -, R 3 = H, M + , m/e 250IIIvif, R 1 = CH 3 , R 2 = COOC 2 H 5 , R 3 = OCH 3 ,M + , m/e 282IIIviiif, R 1 = R 2 = CH 3 , R 3 = OCH 3 , M + , m/e 224IIIixf, R 1 = Ph, R 2 = H, R 3 = H, M + , m/e 272IIIxif, R 1 = 4-OCH 3 Ph, R 2 = R 3 = H, M + , m/e 302IIIxiiif, R 1 = 4-CH 3 Ph, R 2 = R 3 = H, M + , m/e 286IIIxvf, R 1 = 4-BrPh, R 2 = R 3 = H, M + , m/e 351IIIxixf, R 1 = Ph, R 2 = CH 3 , R 3 = H, M + , m/e 286SScheme-24:General fragmentation pattern of condensed pyrimidinylmethylthiobenzimidazoles (IIIi-xxxv) synthesized106
Part-IResults and DiscussionSpecimen IR spectrum of condesed derivatives of substituted 2-chloromethylthienopyrimidinesand 2-mercaptobenzimidazoles.1. IR spectrum of 2-(1H-benzimidazol-2-yl)methylthio-5,6,7,8-tetrahydrobenzo(b)-thieno[2,3-d]pyrimidin-4-(3H)-one IIIi105%T907560453247.273045.703031.232939.612902.002883.682842.202809.412773.732738.052715.861584.571554.681432.191413.871346.361007.84ONHSN1271.131233.521195.911151.54969.26918.15743.58723.33604.70401.2130SNHNC 18H 16N 4OS 2Mol. Wt.: 368.484000JB-21350030002500200017501662.691500125010007505001/cmIR (KBr) cm -1 : 3247(γ NH ), 2939(γ C-H ), 1680(γ CONH ), 743(γ C-S ).Specimen 1 H NMR spectrum of condesed derivatives of substituted 2-chloromethylthienopyrimidinesand 2-mercaptobenzimidazoles.2.1 HNMR spectrum of 2-(1H-benzimidazol-2-yl)methylthio-5,6,7,8-tetrahydrobenzo-(b)thieno[2,3-d]pyrimidin-4-(3H)-one (IIIi)ONHSNSNC 18H 16N 4OS 2Mol. Wt.: 368.48HN107
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Saurashtra UniversityRe - Accredite
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Statement Under O.Ph.D. 7 of Sauras
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ContentsAcknowledgementRegistration
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Contents1.2 Synthesis of condensed
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Contents1.5 MDR modulators 3981.6 D
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infrastructure and all the faciliti
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Above all I thank Lord Hanuman Ji a
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Abbreviations used1 H NMR Proton Nu
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UVVEGFRWCRWHOZ-EUltra VioletVascula
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22. 2-Substitutedthieno[3,2-d]/benz
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PrefacePrefaceHeterocyclic chemistr
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PrefaceThis entire cascade of react
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PrefaceOONHNHPOCl 3MWINVi-xviiClClC
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PrefaceOOHOOOONHNHDP-7 1NHMonastrol
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PART-I
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3.7 Results and discussion on biolo
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Part-1Review on Antiulcer Literatur
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Table 2: Distinguishing Features of
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1.2.2. Muscarinic AntagonistsPart-1
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1.5.5. Pharmacological PropertiesPa
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Page 89 and 90: 2. Aim of the Present WorkPart-IAim
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Page 97 and 98: Part-IAim of Present WorkS. No. A S
Page 99 and 100: 3. Results and Discussion
Page 101 and 102: Part-IResults and Discussion3.1.1d
Page 103 and 104: Part-IResults and DiscussionOR 1XR
Page 105 and 106: Part-IResults and Discussionformed
Page 107 and 108: Part-IResults and DiscussionOOON 2
Page 109 and 110: c. Synthesis of 2-carbethoxy-3-amin
Page 111 and 112: Part-IResults and DiscussionTable 7
Page 113 and 114: Part-IResults and DiscussionOOEtNHO
Page 115 and 116: Part-IResults and DiscussionTable-8
Page 117 and 118: Part-IResults and DiscussionCompd.N
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Page 121 and 122: S. No. Y Mol. Formula(Sol. ofrecrys
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Page 127 and 128: Part-IResults and DiscussionONNHIII
Page 129 and 130: Part-IResults and DiscussionS. No.A
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Page 137 and 138: Specimen 1 H NMR spectra of 2-chlor
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Page 143 and 144: The Infrared (IR) spectra:Part-IRes
Page 145 and 146: Part-IResults and DiscussionR 1ON+
Page 147 and 148: Part-IResults and DiscussionOSNHOSN
Page 149 and 150: 3.6 Biological Evaluation of PPI’
Page 151 and 152: Part-IResults and DiscussionExperim
Page 153 and 154: Part-IResults and DiscussionDrug Pr
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Page 169 and 170: Part-IResults and Discussion2. Effe
Page 171 and 172: Part-IResults and Discussionby kine
Page 173 and 174: Part-IResults and DiscussionNNNNNHN
Page 175 and 176: 3.8. QSAR StudiesPart-IResults and
Page 177 and 178: Part-IResults and DiscussionFigure-
Page 179 and 180: Part-IResults and DiscussionPhysico
Page 183 and 184: Part-IResults and DiscussionThe MDS
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3. Ulcer scoreDescription of the de
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Part-IResults and DiscussionTable-1
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Part-IResults and DiscussionTable-1
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Part-IResults and Discussion24. Ros
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4. Experimental
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Part-IExperimental119 o C was 128-1
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5. Synthesis of ethyl 2-amino-4-phe
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Part-IExperimentalthe procedure des
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Part-IExperimentalRecrystallization
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Part-IExperimentalM.P. : 132-134 o
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Part-IExperimentalA solution of thi
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Part-IExperimentalNMR (CDCl 3 )δpp
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Part-IExperimental6. Reaction of et
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Part-IExperimentalNMR (CDCl 3 )δpp
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Part-IExperimentalM.P. : 240-245 o
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Part-IExperimentalrecrystallization
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Part-IExperimental(1H, d, CH at imi
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Part-IExperimentalNMR (DMSO-d 6 )δ
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M.P. : 140-142 o C; Yield: 73%.Mol.
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M.P. : 135-141 o C; Yield: 67%.Mol.
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Part-IExperimentalml), over a perio
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Part-IExperimentalchloride was adde
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Part-IExperimental29. Synthesis of
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Part-IExperimentalIR (KBr) cm -1 :
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Part-IExperimentaladded while stirr
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Part-IExperimentald]pyrimidin-4(3H)
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Part-IExperimentalMol. formula : C
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Part-IExperimentalthis clear soluti
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Part-IExperimentalwhile maintaining
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Part-IExperimentalMol. Formula : C
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PART-II
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Part-IIContents2.3.2.1 Mononuclear
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Part-IISynthesis of Pyrimidines1. S
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Part-IISynthesis of PyrimidinesYZR
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Part-IISynthesis of Pyrimidineselec
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Part-IISynthesis of PyrimidinesR 1R
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Part-IISynthesis of Pyrimidinespyri
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R 1 R 2 R Yield(%)Part-IISynthesis
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Part-IISynthesis of Pyrimidinesyiel
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Table 27: 2-Amino-3-substitutedaryl
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Part-IISynthesis of PyrimidinesWhil
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Part-IISynthesis of PyrimidinesSimi
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Part-IISynthesis of PyrimidinesTabl
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R 1 R 2 R X Yield(%)Part-IISynthesi
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Part-IISynthesis of Pyrimidines+RCN
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Part-IISynthesis of PyrimidinesNN+
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Part-IISynthesis of PyrimidinesR 1+
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Part-IISynthesis of Pyrimidinesthe
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Part-IISynthesis of Pyrimidinesacet
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Part-IISynthesis of Pyrimidinesexpe
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Part-IISynthesis of PyrimidinesNOOC
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Part-IISynthesis of PyrimidinesThe
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Part-IISynthesis of PyrimidinesTabl
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Part-IISynthesis of PyrimidinesOH 3
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1.10 ReferencesPart-IISynthesis of
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Part-IISynthesis of Pyrimidines42.
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2. Impact of Microwave Assisted Hea
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Part-IIImpact of Microwave…Microw
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Part-IIImpact of Microwave…Figure
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Part-IIImpact of Microwave…R 1ArR
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Part-IIImpact of Microwave…as an
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Part-IIImpact of Microwave…al. 21
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Part-IIImpact of Microwave…XOHR 1
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Part-IIImpact of Microwave…N+N21B
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Part-IIImpact of Microwave…OO+ NO
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Part-IIImpact of Microwave…NO 2NO
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Part-IIImpact of Microwave…RNHNNH
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Part-IIImpact of Microwave…assist
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Part-IIImpact of Microwave…CNRNH
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Part-IIImpact of Microwave…Multig
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Part-IIImpact of Microwave…Nie et
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Part-IIImpact of Microwave…synthe
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Part-IIImpact of Microwave…An eff
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Part-IIImpact of Microwave…OO+S 8
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2.6. ReferencesPart-IIImpact of Mic
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49. Baxendale, I. R.; Ley, S. V. J.
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Part-IIAim of the Present Work3. Ai
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Part-IIAim of the Present WorkONHR
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Part-IIAim of the Present WorkYZXNN
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Part-IIAim of the Present WorkThe c
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3.5 References:Part-IIAim of the Pr
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Part-IIAim of the Present Work37. S
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Part-IIResults and Discussion4.1 Sy
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4.2 Synthesis of condensed 2-substi
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Table 38: Physical data of condense
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S. No. X Time ofMWIHeating(Min)VxiV
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S. No. X Time ofMWIHeating(Min)Yiel
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4.3 Synthesis of condensed 4-chloro
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Part-IIResults and DiscussionHerein
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Part-IIResults and DiscussionS. No.
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Part-IIResults and DiscussionS. No.
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The Mass spectraPart-IIResults and
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Specimen IR spectra of some 2-chlor
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Part-IIResults and Discussion1 H NM
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Part-IIResults and Discussionion (c
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Specimen 1 H NMR spectra of 4-chlor
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Part-IIResults and Discussion4.5 MD
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Part-IIResults and DiscussionH 3CO1
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Part-IIResults and DiscussionCl14.
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Part-IIResults and DiscussionO14. V
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4.6 References:Part-IIResults and D
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5. ExperimentalPart-IIExperimentalA
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3. Synthesis of 2-chloromethyl-5-ph
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Part-IIExperimentalIR (KBr) cm -1 :
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Part-IIExperimentalM.P. : 247-249 o
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Part-IIExperimental5.4 Synthesis of
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Part-IIExperimentalwere reacted und
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27. Synthesis of 2-methyl-5-phenylt
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Part-IIExperimental80 o C) that yie
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Part-IIExperimental36. Synthesis of
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Part-IIExperimentalunder microwave
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Part-IIExperimentalM.P. : >300 o C
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M.P. : 280-282 o C; Yield: 90%Mol.
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5.10 References:Part-IIExperimental
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Synthesis, Characterization and Ant
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Part-IIIAdvances Dihydropyridines a
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CH 3CH 3Part-IIIAdvances Dihydropyr
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2. Aim of the Present Work
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Part-IIIAim of the Present Workshor
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3. Results and Discussion
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Part-IIIResults and DiscussionOOOHR
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Part-IIIResults and DiscussionUsing
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Part-IIIResults and DiscussionS. No
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S. No R X MolFormula(Sol. of Recrys
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Part-IIIResults and Discussionpheny
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Specimen 13 C NMR spectra of some D
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Part-IIIResults and DiscussionTable
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Part-IIIResults and DiscussionTable
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3.5 DiscussionPart-IIIResults and D
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4. Experimental
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Part-IIIExperimentalglacial acetic
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Part-IIIExperimental5. Synthesis of
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Part-IIIExperimentalIR(KBr) cm -1 :
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Part-IIIExperimentalM.P. : 184-186
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Part-IIIExperimental1 H NMR(DMSO-d
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Part-IIIExperimentalM.P. : 188-190
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Part-IIIExperimental4.2 MDR reversa
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Summary and Conclusion
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Summary and Conclusionactivity in P
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Summary and Conclusionreverting act
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Publications and Presentations
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Publications and PresentationsOther
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Publications and Presentations8. K.
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