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produção de micropartículas e nanopartículas poliméricas ... - UFRJ

produção de micropartículas e nanopartículas poliméricas ... - UFRJ

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Filename: C:\Program Files\Py...\amostra12(marco).dsd<br />

Operator ID: Grazielle<br />

Sample ID: amostra12(marco)<br />

Sample Weight: 20.190 mg<br />

Comment:<br />

Heat Flow Endo Up (mW)<br />

30<br />

28<br />

26<br />

24<br />

22<br />

20<br />

18<br />

16<br />

1) Hold for 1.0 min at -20.00°C<br />

2) Heat from -20.00°C to 140.00°C at 10.00°C/min<br />

3) Cool from 140.00°C to -20.00°C at 100.00°C/min<br />

PerkinElmer Thermal Analysis<br />

Tg: Half Cp Extrapolated = 41.18 °C<br />

Onset = 37.48 °C<br />

Delta Cp = 0.700 J/g*°C<br />

-20 0 20 40 60 80 100 120 140<br />

Temperature (°C)<br />

4) Hold for 3.0 min at -20.00°C<br />

5) Heat from -20.00°C to 140.00°C at 10.00°C/min<br />

Figura A11 – Curva <strong>de</strong> DSC do PVAc + 0,5% amoxicilina (fase aquosa).<br />

1/15/2009 3:27:09 PM<br />

260

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