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produção de micropartículas e nanopartículas poliméricas ... - UFRJ

produção de micropartículas e nanopartículas poliméricas ... - UFRJ

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Filename: C:\Program Files\Py...\amostra14(marco).dsd<br />

Operator ID: Grazielle<br />

Sample ID: amostra14(marco)<br />

Sample Weight: 17.090 mg<br />

Comment:<br />

Heat Flow Endo Up (mW)<br />

35<br />

34<br />

32<br />

30<br />

28<br />

26<br />

24<br />

22<br />

20<br />

18<br />

16<br />

14<br />

12<br />

10<br />

1) Hold for 1.0 min at -20.00°C<br />

2) Heat from -20.00°C to 140.00°C at 10.00°C/min<br />

3) Cool from 140.00°C to -20.00°C at 100.00°C/min<br />

PerkinElmer Thermal Analysis<br />

Onset = 48.95 °C<br />

Tg: Half Cp Extrapolated = 54.99 °C<br />

Delta Cp = 0.202 J/g*°C<br />

-19.97 0 20 40 60 80 100 120 140<br />

Temperature (°C)<br />

4) Hold for 3.0 min at -20.00°C<br />

5) Heat from -20.00°C to 140.00°C at 10.00°C/min<br />

1/28/2009 2:54:47 PM<br />

Figura A16 – Curva <strong>de</strong> DSC do PVAc-co-PMMA + 1,0% amoxicilina (fase orgânica).<br />

22.8<br />

22<br />

20<br />

18<br />

16<br />

14<br />

12<br />

10<br />

8<br />

6<br />

4<br />

2<br />

0<br />

-2<br />

Derivative Heat Flow (mW/min)<br />

-2.653<br />

265

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