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Pulacayo Project Feasibility Study - Apogee Silver

Pulacayo Project Feasibility Study - Apogee Silver

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<strong>Pulacayo</strong> 1 000 t/d Phase I <strong>Feasibility</strong> <strong>Study</strong> - NI 43-101 Technical Report<br />

090644-3-0000-20-IFI-100<br />

on project samples. <strong>Project</strong> analytical work has been completed by ALS at its analytical<br />

facility in Lima, Peru after completion of sample preparation procedures at the ALS facility<br />

located in Oruro Bolivia. ALS is an internationally accredited laboratory with National<br />

Association of Testing Authorities (NATA) certification and also complies with standards of<br />

ISO 9001:2000 and ISO 17025:1999. The laboratory utilizes industry standard analytical<br />

methodology and utilizes rigorous internal Quality Assurance and Quality Control (QAQC)<br />

procedures for self-testing.<br />

All samples are weighed upon receipt at the lab and prepared using ALS preparation<br />

procedure PREP-31B that consists of crushing the entire sample to >70% -2 mm, then<br />

splitting off 1 kg and pulverizing it to better than 85% passing 75 micron. The coarse reject<br />

materials from this processing are returned to <strong>Apogee</strong> for storage on site at <strong>Pulacayo</strong>. Similar<br />

processing was used by ASC.<br />

<strong>Silver</strong>, lead and zinc concentrations for <strong>Apogee</strong> programs were analyzed by ALS using an<br />

Aqua Regia digestion and Atomic Absorption Spectroscopy (AAS) following ALS method<br />

codes AA46 and AA62. Samples returning assay values greater than 300 g/t Ag were further<br />

analyzed using quantitative method Ag-GRAV22, which uses a Fire Assay pre-concentration<br />

and Gravimetric Finish on a 50 g sample aliquot. Gold values were determined using the Au-<br />

AA26 analytical method provided by ALS that employs a Fire Assay pre-concentration<br />

followed by Atomic Absorption finish on a 50 g sample aliquot. A 35 element multi-element<br />

analysis was also completed on samples using method code ME-ICP41 that uses Aqua<br />

Regia digestion and ICP-AES analysis.<br />

11.4 Drill Core Analysis from 2002 to 2003 ASC Programs<br />

Samples from the ASC drilling programs carried out in 2002 and 2003 were also prepared<br />

and analyzed by ALS. However, after preparation at the facility in Oruro, Bolivia under the<br />

same protocols as noted above for <strong>Apogee</strong>, analytical work was carried out at the company`s<br />

laboratory in Vancouver, BC, Canada. This facility is fully accredited, as described earlier and<br />

analytical protocols were the same as those described above for <strong>Apogee</strong>.<br />

11.5 Quality Assurance and Control from 2006 to 2012 <strong>Apogee</strong> Programs<br />

<strong>Apogee</strong> developed an internal QAQC program that includes blind insertion of reference<br />

standards, blanks and duplicates in each analytical shipment. A blank is inserted at the<br />

beginning of each sample batch, standards are inserted at random intervals throughout each<br />

batch of 50 samples and duplicates are analyzed at the end of each batch. All data gathered<br />

for QAQC purposes is captured, sorted and retained in the QAQC database. <strong>Apogee</strong><br />

purchased two commercial reference standards from Western Canadian Minerals Ltd.<br />

(WCM), these being PB-128 and PB-124, created an in-house standard and also purchased<br />

commercial prepared blank materials. Coarse field blanks were prepared by <strong>Apogee</strong> from<br />

locally sourced un-mineralized quartzite outcropping near <strong>Pulacayo</strong>.<br />

Three quality control samples that include a field or commercial blank, a commercial standard<br />

and a duplicate sample are inserted with a minimum frequency of 1 in every 50 samples.<br />

Review by Mercator showed that in practice, an analytical standard typically occurs within<br />

every 20 samples submitted for analysis. Analysis of duplicate samples of quarter core is<br />

TWP Sudamérica S.A. Av. Encalada 1257 Of. 801, Santiago de Surco Lima 33, Perú (51-1) 4377473<br />

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