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Tecnai on-line help manual -- Options - UT Southwestern

Tecnai on-line help manual -- Options - UT Southwestern

Tecnai on-line help manual -- Options - UT Southwestern

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<str<strong>on</strong>g>Tecnai</str<strong>on</strong>g> <strong>on</strong>-<strong>line</strong> <strong>help</strong> Opti<strong>on</strong>s 98Opti<strong>on</strong>s Software versi<strong>on</strong> 2Angular Error LimitThe angular error limit determines by how much the interplanar angle between the two d-spacingscalculated may differ from the measured angle.OKPressing OK exits the match c<strong>on</strong>straints dialog while keeping any changes made to the values of thematch c<strong>on</strong>straints.CancelPressing Cancel exits the match c<strong>on</strong>straints dialog without changing the values of the match c<strong>on</strong>straints.7.6 Two-z<strong>on</strong>e indexing procedure in stepsThe two-z<strong>on</strong>e indexing procedure can be executed as follows:• Find a suitable first z<strong>on</strong>e <strong>on</strong> the crystal with the stage tilts.Intermezzo: Making it easier to find a suitable sec<strong>on</strong>d z<strong>on</strong>e axis• Identify the z<strong>on</strong>e axis and use the Manual indexing method to set the rough orientati<strong>on</strong> of the crystal.• Store the stage positi<strong>on</strong> in the Stage c<strong>on</strong>trol panel.• Change the orientati<strong>on</strong> to a different z<strong>on</strong>e axis <strong>on</strong> the k-Space display.• Press the Stage To butt<strong>on</strong> in the k-Space C<strong>on</strong>trol Panel to tilt the real crystal to the new orientati<strong>on</strong>.• Adjust the stage tilts to bring the required z<strong>on</strong>e axis to the center.• Store this stage positi<strong>on</strong> also in the Stage c<strong>on</strong>trol panel.• Go back to the stored positi<strong>on</strong> for the first z<strong>on</strong>e axis with the Move To or Go To functi<strong>on</strong> of the stage.• When the sec<strong>on</strong>d z<strong>on</strong>e axis is needed, use the same functi<strong>on</strong>s to recall that stage positi<strong>on</strong>.End of intermezzo• Press the 2-Z<strong>on</strong>e butt<strong>on</strong> in the Crystal tab of the flap-out of the k-Space C<strong>on</strong>trol panel.• In the Two Z<strong>on</strong>e Indexing dialog, select a z<strong>on</strong>e-axis memory for the primary z<strong>on</strong>e axis with the spinbutt<strong>on</strong>s and press Calculator for the Primary z<strong>on</strong>e axis.

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