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official journal of the patent office - Controller General of Patents ...

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(12) PATENT APPLICATION PUBLICATION<br />

(19) INDIA (21) Application No.: 00088/KOL/2004 A<br />

(22) Date <strong>of</strong> filing <strong>of</strong> Application: 03.03.2004 (43) Publication Date: 09/06/2006<br />

(54) Title <strong>of</strong> <strong>the</strong> invention: CATALYST, PROCESS FOR PRODUCING THE CATALYST AND PROCESS FOR PREPARING<br />

VINYL ACETATE USING THE CATALYST<br />

(51) International classification : B01J 37/02, 21/08,<br />

23/44, 23/52<br />

(31) Priority Document No : 19754992.6<br />

(32) Priority Date : 11.12.1997<br />

(33) Name <strong>of</strong> priority country : GERMANY<br />

(86) International Application No and : NA<br />

Filing Date<br />

:<br />

(87) International Publication No : NA<br />

(61) Patent <strong>of</strong> addition to Application No : NA<br />

Filed on : NA<br />

(62) Divisional to Application No : 2020/CAL/1998<br />

Filed on : 16/11/1998<br />

(71) Name <strong>of</strong> Applicant:<br />

CELANESE GMBH<br />

Address <strong>of</strong> <strong>the</strong> Applicant:<br />

LURGIALLEE 14, D-60439 FRANKFURT,<br />

FEDERAL REPUBLIC OF GERMANY<br />

(72) Name <strong>of</strong> <strong>the</strong> Inventor:<br />

BERNHARD HERZOG<br />

Filed U/S 5(2) before The <strong>Patents</strong> (Amendment)<br />

Act, 2005: NO<br />

(57) Abstract:<br />

The present process allows <strong>the</strong> production <strong>of</strong> a catalyst for preparing vinyl acetate in <strong>the</strong> gas phase from ethylene, acetic acid and<br />

oxygen or oxygen-containing gases. The catalyst comprises palladium and/or its compounds, gold and/or its compounds and also<br />

alkali metal compounds on a particulate, porous support, and is produced by<br />

a) impregnating <strong>the</strong> support with soluble palladium and gold compounds,<br />

b) converting <strong>the</strong> soluble palladium and gold compounds into insoluble palladium and gold compounds by addition <strong>of</strong> an<br />

alkaline solution to <strong>the</strong> support,<br />

C) reducing <strong>the</strong> insoluble palladium and gold compounds on <strong>the</strong> support by means <strong>of</strong> a reducing agent in <strong>the</strong> liquid or<br />

gaseous phase,<br />

d) impregnating <strong>the</strong> support with at least one soluble alkali metal compound and<br />

e) finally drying <strong>the</strong> Support at a maximum <strong>of</strong> 150 0 C,<br />

wherein <strong>the</strong> catalyst is irradiated with microwaves before , during or after one <strong>of</strong> <strong>the</strong> process steps a) to e).<br />

(FIG.nil)<br />

The Patent Office Journal 09/06/2006 10954

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